2-phenyl-1-((2S,6S)-6-((E)-prop-1-en-1-yl)tetrahydro-2H-pyran-2-yl)ethanone

Base Information

Chemical Name:2-phenyl-1-((2S,6S)-6-((E)-prop-1-en-1-yl)tetrahydro-2H-pyran-2-yl)ethanone
CAS No.:1449224-65-0
Molecular Formula:C₁₆H₂₀O₂
Molecular Weight:244.334
Hs Code.:

Synonyms:

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Chemical Property of 2-phenyl-1-((2S,6S)-6-((E)-prop-1-en-1-yl)tetrahydro-2H-pyran-2-yl)ethanone

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Technology Process of 2-phenyl-1-((2S,6S)-6-((E)-prop-1-en-1-yl)tetrahydro-2H-pyran-2-yl)ethanone

There total 8 articles about 2-phenyl-1-((2S,6S)-6-((E)-prop-1-en-1-yl)tetrahydro-2H-pyran-2-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₆O

: 1449224-65-0
2-phenyl-1-((2S,6S)-6-((E)-prop-1-en-1-yl)tetrahydro-2H-pyran-2-yl)ethanone

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / tetrahydrofuran / 0 °C / Inert atmosphere

2: disodium ethylenediaminetetraacetic acid; potassium carbonate; Oxone; borax; tetra(n-butyl)ammonium hydrogensulfate / water; acetonitrile / 0 °C / Inert atmosphere

3: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere

4: perrhenic acid anhydride / dichloromethane / 36 h / 20 °C / Inert atmosphere

5: silica gel; pyridinium chlorochromate / dichloromethane / Inert atmosphere

With borax; Oxone; perrhenic acid anhydride; tetra(n-butyl)ammonium hydrogensulfate; silica gel; disodium ethylenediaminetetraacetic acid; sodium hydride; diisobutylaluminium hydride; potassium carbonate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201208132

Reference yield:

: C₁₆H₂₀O

: 1449224-65-0
2-phenyl-1-((2S,6S)-6-((E)-prop-1-en-1-yl)tetrahydro-2H-pyran-2-yl)ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: disodium ethylenediaminetetraacetic acid; potassium carbonate; Oxone; borax; tetra(n-butyl)ammonium hydrogensulfate / water; acetonitrile / 0 °C / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere

3: perrhenic acid anhydride / dichloromethane / 36 h / 20 °C / Inert atmosphere

4: silica gel; pyridinium chlorochromate / dichloromethane / Inert atmosphere

With borax; Oxone; perrhenic acid anhydride; tetra(n-butyl)ammonium hydrogensulfate; silica gel; disodium ethylenediaminetetraacetic acid; diisobutylaluminium hydride; potassium carbonate; pyridinium chlorochromate; In dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201208132

Reference yield:

: 1449224-49-0
(E)-7-((2R,3R)-3-benzyloxiran-2-yl)hept-3-en-2-ol

: 1449224-65-0
2-phenyl-1-((2S,6S)-6-((E)-prop-1-en-1-yl)tetrahydro-2H-pyran-2-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: perrhenic acid anhydride / dichloromethane / 36 h / 20 °C / Inert atmosphere

2: silica gel; pyridinium chlorochromate / dichloromethane / Inert atmosphere

With perrhenic acid anhydride; silica gel; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/anie.201208132