C₂₆H₁₉ClN₄O

Base Information

• Chemical Name: C₂₆H₁₉ClN₄O
• CAS No.: 1374460-73-7
• Molecular Formula: C₂₆H₁₉ClN₄O
• Molecular Weight: 438.916
• Mol file: 1374460-73-7.mol

Synonyms:

Chemical Property of C₂₆H₁₉ClN₄O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₁₉ClN₄O

There total 4 articles about C₂₆H₁₉ClN₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-(4-chlorophenyl)-1H-benzimidazol-1-yl)-acetic acid ethyl ester (705970-56-5) → C26H19ClN4O (1374460-73-7)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 4 h / Reflux

2: ammonium cerium (IV) nitrate / ethanol / 0.5 h / Reflux

With ammonium cerium (IV) nitrate; hydrazine hydrate; In ethanol;

DOI:10.1111/j.1747-0285.2012.01347.x

Reference yield:

1,2-diamino-benzene (95-54-5) → C26H19ClN4O (1374460-73-7)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium metabisulfite

2: potassium hydroxide / dimethyl sulfoxide

3: hydrazine hydrate / ethanol / 4 h / Reflux

4: ammonium cerium (IV) nitrate / ethanol / 0.5 h / Reflux

With sodium metabisulfite; ammonium cerium (IV) nitrate; hydrazine hydrate; potassium hydroxide; In ethanol; dimethyl sulfoxide;

DOI:10.1111/j.1747-0285.2012.01347.x

Reference yield:

4-chlorobenzaldehyde (104-88-1) → C26H19ClN4O (1374460-73-7)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium metabisulfite

2: potassium hydroxide / dimethyl sulfoxide

3: hydrazine hydrate / ethanol / 4 h / Reflux

4: ammonium cerium (IV) nitrate / ethanol / 0.5 h / Reflux

With sodium metabisulfite; ammonium cerium (IV) nitrate; hydrazine hydrate; potassium hydroxide; In ethanol; dimethyl sulfoxide;

DOI:10.1111/j.1747-0285.2012.01347.x

upstream raw materials:

(2-(4-chlorophenyl)-1H-benzimidazol-1-yl)-acetic acid ethyl ester

1-naphthaldehyde

4-chlorobenzaldehyde

1,2-diamino-benzene

Downstream raw materials:

C₂₈H₂₁ClN₄O₂S