1-Triphenylsilyl-1-methoxy-aethanan

Base Information

• Chemical Name: 1-Triphenylsilyl-1-methoxy-aethanan
• CAS No.: 24337-33-5
• Molecular Formula: C₂₁H₂₀OSi
• Molecular Weight: 316.475
• Mol file: 24337-33-5.mol

Synonyms:

Chemical Property of 1-Triphenylsilyl-1-methoxy-aethanan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Triphenylsilyl-1-methoxy-aethanan

There total 3 articles about 1-Triphenylsilyl-1-methoxy-aethanan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methoxyethene (107-25-5,9003-09-2) + Triphenylsilyl chloride (76-86-8) → 1-Triphenylsilyl-1-methoxy-aethanan (24337-33-5)

Guidance literature:

With tert.-butyl lithium; In tetrahydrofuran; pentane;

DOI:10.1016/S0040-4039(00)82072-9

Reference yield:

<α,α-Dimethoxy-aethyl>-triphenylsilan (24337-29-9) → 1-Triphenylsilyl-1-methoxy-aethanan (24337-33-5)

Guidance literature:

at 140 ℃;

DOI:10.1139/v69-719

Reference yield:

(2-methyl-[1,3]dithian-2-yl)-triphenyl-silane (13433-56-2) → 1-Triphenylsilyl-1-methoxy-aethanan (24337-33-5)

Guidance literature:

Multi-step reaction with 2 steps

1: HgO, HgCl₂, CdCO₃ / Ambient temperature

2: 140 °C

With cadmium(II) carbonate; mercury dichloride; mercury(II) oxide;

DOI:10.1139/v69-719

upstream raw materials:

<α,α-Dimethoxy-aethyl>-triphenylsilan

methoxyethene

Triphenylsilyl chloride

(2-methyl-[1,3]dithian-2-yl)-triphenyl-silane

Downstream raw materials:

Acetyltriphenylsilane