C₃₆H₃₆F₃N₃O₁₀

Base Information

Chemical Name:C₃₆H₃₆F₃N₃O₁₀
CAS No.:1361928-15-5
Molecular Formula:C₃₆H₃₆F₃N₃O₁₀
Molecular Weight:727.691
Hs Code.:

C<sub>36</sub>H<sub>36</sub>F<sub>3</sub>N<sub>3</sub>O<sub>10</sub>

Synonyms:

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Chemical Property of C₃₆H₃₆F₃N₃O₁₀

Chemical Property:

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Technology Process of C₃₆H₃₆F₃N₃O₁₀

There total 10 articles about C₃₆H₃₆F₃N₃O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361928-06-4
1-(2'-O-acetyl-3',5'-di-O-benzyl-4'-C-azidomethyl-β-D-ribofuranosyl)-3-(4-methoxybenzyl)uracil

: 1361928-15-5
C₃₆H₃₆F₃N₃O₁₀

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium methylate / methanol / 3 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

3.1: ammonium cerium (IV) nitrate / water; acetonitrile / 55 h / 20 °C

4.1: water; triphenylphosphine / tetrahydrofuran / 4 h / 45 °C

5.1: triethylamine / tetrahydrofuran / 0 - 20 °C

6.1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 70 °C

7.1: pyridine / 24 h / 20 °C

8.1: pyridine / 20 °C

With ammonium cerium (IV) nitrate; palladium 10% on activated carbon; water; hydrogen; sodium methylate; sodium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; pyridine; methanol; ethanol; water; acetonitrile;
DOI:10.1021/jo202666m

Reference yield:

: 1361928-07-5
C₃₂H₃₃N₅O₇

: 1361928-15-5
C₃₆H₃₆F₃N₃O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: ammonium cerium (IV) nitrate / water; acetonitrile / 55 h / 20 °C

3.1: water; triphenylphosphine / tetrahydrofuran / 4 h / 45 °C

4.1: triethylamine / tetrahydrofuran / 0 - 20 °C

5.1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 70 °C

6.1: pyridine / 24 h / 20 °C

7.1: pyridine / 20 °C

With ammonium cerium (IV) nitrate; palladium 10% on activated carbon; water; hydrogen; sodium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; pyridine; ethanol; water; acetonitrile;
DOI:10.1021/jo202666m

Reference yield:

: C₂₅H₂₉N₃O₆

: 1361928-15-5
C₃₆H₃₆F₃N₃O₁₀

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 70 °C

3: pyridine / 24 h / 20 °C

4: pyridine / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; pyridine; ethanol;
DOI:10.1021/jo202666m