ortho-tolyltrichloro germane

Base Information

Chemical Name:ortho-tolyltrichloro germane
CAS No.:155728-49-7
Molecular Formula:C₇H₇Cl₃Ge
Molecular Weight:270.082
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ortho-tolyltrichloro germane

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Technology Process of ortho-tolyltrichloro germane

There total 1 articles about ortho-tolyltrichloro germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 10038-98-9
germaniumtetrachloride

: 108-88-3,15644-74-3,16713-13-6
toluene

: 155728-49-7
ortho-tolyltrichloro germane

: 19089-95-3
(4-methylphenyl)trichlorogermane

Guidance literature:: aluminium trichloride; In neat (no solvent); other Radiation; a mixt. of toluene, GeCl4 and powdered AlCl3 as catalyst is placed in aPyrex tube with N2 bubbling, 300-W microwave power is applied for 15 min, AlCl3 is added once more and the mixt. is refluxed for 1 h (Ar); mixt. is treated with POCl3 and filtered, mixt. of isomers (ratio 90:10) is isolated;
DOI:10.1021/om00018a050