Technology Process of C56H98N10O14Si2
There total 12 articles about C56H98N10O14Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: HOBt; EDC; DIPA / tetrahydrofuran
2: HCl / tetrahydrofuran
3: NaBH(OAc)3; AcOH / tetrahydrofuran / 20 °C
4: H2 / 10 percent Pd/C / methanol / 20 °C / atmospheric pressure
5: HOBt; EDC; Hunig base / tetrahydrofuran / 20 °C
6: H2; AcOH / 10 percent Pd/C / methanol
With
hydrogenchloride; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; diisopropylamine; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00671-1
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: LDA / tetrahydrofuran / 1 h / -78 °C
1.2: 31 percent / tetrahydrofuran / 17 h / -78 - -35 °C
2.1: H2 / 10 percent Pd/C / methanol
3.1: NaBH(OAc)3; AcOH / tetrahydrofuran / 20 °C
4.1: H2 / 10 percent Pd/C / methanol / 20 °C / atmospheric pressure
5.1: HOBt; EDC; Hunig base / tetrahydrofuran / 20 °C
6.1: H2; AcOH / 10 percent Pd/C / methanol
With
hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00671-1
