HOs₃(CH₃OCCC₆H₅CC₆H₅)(CO)9

Base Information

• Chemical Name: HOs₃(CH₃OCCC₆H₅CC₆H₅)(CO)9
• CAS No.: 97689-39-9
• Molecular Formula: C₂₅H₁₄O₁₀Os₃
• Molecular Weight: 1044.98
• Mol file: 97689-39-9.mol

Synonyms:

Chemical Property of HOs₃(CH₃OCCC₆H₅CC₆H₅)(CO)9

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of HOs₃(CH₃OCCC₆H₅CC₆H₅)(CO)9

There total 1 articles about HOs₃(CH₃OCCC₆H₅CC₆H₅)(CO)9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

HOs3(CO)10(COMe) + diphenyl acetylene (501-65-5) → HOs3(CH3OCCC6H5CC6H5)(CO)9 (97689-39-9)

Guidance literature:

In toluene; a soln. of the cluster and of the alkyne in molar ratio 0.059:0.23 placing in a NMR tube; heating under N2 at 95°C for 106 h (NMR monitoring); solvent removing, chromy. on SiO2; identified by IR, NMR and mass spectra;

DOI:10.1021/om00129a004

Reference yield:

HOs3(CH3OCCC6H5CC6H5)(CO)9 (97689-39-9) → H4Os4(CO)12 (12375-04-1)

Guidance literature:

With hydrogen; In not given;

DOI:10.1021/om00129a004

upstream raw materials:

diphenyl acetylene

Downstream raw materials:

H₄Os₄(CO)12

Refernces