Technology Process of C32H37N3O7
There total 8 articles about C32H37N3O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: cobalt(II) chloride hexahydrate / aq. phosphate buffer / 120 h / 40 °C / Enzymatic reaction
2.1: cobalt(II) chloride hexahydrate / aq. phosphate buffer / 168 h / 40 °C / Enzymatic reaction
3.1: sodium carbonate / 1,4-dioxane; water / 6 h / 0 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C
5.1: tetrahydrofuran / 6 h / 50 °C
6.1: triethylamine / N,N-dimethyl-formamide / 1 h / 0 - 20 °C
6.2: 20 °C
7.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C
7.2: 6 °C
8.1: trifluoroacetic acid / dichloromethane
With
cobalt(II) chloride hexahydrate; sodium carbonate; caesium carbonate; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c5ob02145f
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: cobalt(II) chloride hexahydrate / aq. phosphate buffer / 168 h / 40 °C / Enzymatic reaction
2.1: sodium carbonate / 1,4-dioxane; water / 6 h / 0 - 20 °C
3.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C
4.1: tetrahydrofuran / 6 h / 50 °C
5.1: triethylamine / N,N-dimethyl-formamide / 1 h / 0 - 20 °C
5.2: 20 °C
6.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C
6.2: 6 °C
7.1: trifluoroacetic acid / dichloromethane
With
cobalt(II) chloride hexahydrate; sodium carbonate; caesium carbonate; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c5ob02145f