2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione

Base Information

Chemical Name:2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione
CAS No.:154344-34-0
Molecular Formula:C₁₅H₁₄N₂S₂
Molecular Weight:286.422
Hs Code.:

Synonyms:

Suppliers and Price of 2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione

There total 20 articles about 2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65282-42-0
1,2-dithiolo<5,4-b>pyridin-3-one

: 154344-34-0
2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione

Guidance literature:: Multi-step reaction with 35 steps

1: ethanol / Heating

2: I₂; NaHCO₃ / ethanol

3: Lawesson's reagent / toluene / 0.5 h / Heating

4: H₂S / ethanol / pH 7.4

5: I₂; NaHCO₃ / ethanol

6: Hg(OAc)2; AcOH / CHCl₃ / 0.5 h / 20 °C

7: H₂S / ethanol / pH 7.4

8: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating

9: ethanol / Heating

10: I₂; NaHCO₃ / ethanol

11: Lawesson's reagent / toluene / 0.5 h / Heating

12: Hg(OAc)2; AcOH / CHCl₃ / 0.5 h / 20 °C

13: H₂S / ethanol / pH 7.4

14: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating

15: ethanol / Heating

16: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating

17: ethanol / Heating

18: I₂; NaHCO₃ / ethanol

19: Lawesson's reagent / toluene / 0.5 h / Heating

20: Hg(OAc)2; AcOH / CHCl₃ / 0.5 h / 20 °C

21: H₂S / ethanol / pH 7.4

22: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating

23: ethanol / Heating

24: I₂; NaHCO₃ / ethanol

25: Lawesson's reagent / toluene / 0.5 h / Heating

26: H₂S / ethanol / pH 7.4

27: I₂; NaHCO₃ / ethanol

28: Hg(OAc)2; AcOH / CHCl₃ / 0.5 h / 20 °C

29: H₂S / ethanol / pH 7.4

30: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating

31: ethanol / Heating

32: I₂; NaHCO₃ / ethanol

33: Lawesson's reagent / toluene / 0.5 h / Heating

34: H₂S / ethanol / pH 7.4

35: I₂; NaHCO₃ / ethanol

With Lawessons reagent; hydrogen sulfide; mercury(II) diacetate; iodine; sodium hydrogencarbonate; acetic acid; In ethanol; chloroform; toluene;
DOI:10.1016/S0014-827X(00)00084-7

Reference yield:

: 91859-66-4
2-benzylisothiazolo<5,4-b>pyridin-3(2H)-one

: 154344-34-0
2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione

Guidance literature:: Multi-step reaction with 17 steps

1: Lawesson's reagent / toluene / 0.5 h / Heating

2: Hg(OAc)2; AcOH / CHCl₃ / 0.5 h / 20 °C

3: H₂S / ethanol / pH 7.4

4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating

5: ethanol / Heating

6: I₂; NaHCO₃ / ethanol

7: Lawesson's reagent / toluene / 0.5 h / Heating

8: H₂S / ethanol / pH 7.4

9: I₂; NaHCO₃ / ethanol

10: Hg(OAc)2; AcOH / CHCl₃ / 0.5 h / 20 °C

11: H₂S / ethanol / pH 7.4

12: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating

13: ethanol / Heating

14: I₂; NaHCO₃ / ethanol

15: Lawesson's reagent / toluene / 0.5 h / Heating

16: H₂S / ethanol / pH 7.4

17: I₂; NaHCO₃ / ethanol

With Lawessons reagent; hydrogen sulfide; mercury(II) diacetate; iodine; sodium hydrogencarbonate; acetic acid; In ethanol; chloroform; toluene;
DOI:10.1016/S0014-827X(00)00084-7

Reference yield:

: 154344-42-0
2-propylisothiazolo<5,4-b>pyridin-3(2H)-one

: 154344-34-0
2-(3-phenylpropyl)isothiazolo<5,4-b>pyridine-3(2H)-thione

Guidance literature:: Multi-step reaction with 11 steps

1: Lawesson's reagent / toluene / 0.5 h / Heating

2: H₂S / ethanol / pH 7.4

3: I₂; NaHCO₃ / ethanol

4: Hg(OAc)2; AcOH / CHCl₃ / 0.5 h / 20 °C

5: H₂S / ethanol / pH 7.4

6: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating

7: ethanol / Heating

8: I₂; NaHCO₃ / ethanol

9: Lawesson's reagent / toluene / 0.5 h / Heating

10: H₂S / ethanol / pH 7.4

11: I₂; NaHCO₃ / ethanol

With Lawessons reagent; hydrogen sulfide; mercury(II) diacetate; iodine; sodium hydrogencarbonate; acetic acid; In ethanol; chloroform; toluene;
DOI:10.1016/S0014-827X(00)00084-7