chir-anti-{RuCl₂(d-C₁₆H₂₀P₂)2}

Base Information

Chemical Name:chir-anti-{RuCl₂(d-C₁₆H₂₀P₂)2}
CAS No.:39162-64-6
Molecular Formula:C₃₂H₄₀Cl₂P₄Ru
Molecular Weight:720.541
Hs Code.:

chir-anti-{RuCl<sub>2</sub>(d-C<sub>16</sub>H<sub>20</sub>P<sub>2</sub>)2}

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Chemical Property of chir-anti-{RuCl₂(d-C₁₆H₂₀P₂)2}

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Technology Process of chir-anti-{RuCl₂(d-C₁₆H₂₀P₂)2}

There total 1 articles about chir-anti-{RuCl₂(d-C₁₆H₂₀P₂)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14898-67-0
ruthenium trichloride hydrate

: 17325-53-0,17325-54-1,23808-01-7,39480-15-4,90898-69-4
d-1,2-bis-(methylphenylphosphino)-ethane

: 39162-64-6,17168-62-6,17168-60-4,18583-04-5,18583-05-6,17168-61-5
chir-anti-{RuCl₂(d-C₁₆H₂₀P₂)2}

Guidance literature:: With hydrazine hydrate; In methanol; water; a soln. of 14 mmol d-diphosphine and 7 mmol RuCl3*xH2O in 250 ml methanol is treated with a hot aq. soln. of 1 g hydrazine hydrate for 6 h at ambient temp.; all operations under N2-atmosphere;; evapn. in vacuum; the residue is chromd. over silicagel (CHCl3), yielding a unitary (thin-layer chromy.) yellow compound; recrystn. from ligroine, pentane or cyclohexane;;