C₂₆H₃₃OPSi

Base Information

Chemical Name:C₂₆H₃₃OPSi
CAS No.:1402909-66-3
Molecular Formula:C₂₆H₃₃OPSi
Molecular Weight:420.607
Hs Code.:

Synonyms:

Suppliers and Price of C₂₆H₃₃OPSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₃₃OPSi

Chemical Property:

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Technology Process of C₂₆H₃₃OPSi

There total 5 articles about C₂₆H₃₃OPSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21210-43-5
(S)-Methyl mandelate

: 1402909-66-3
C₂₆H₃₃OPSi

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C

2: diisobutylaluminium hydride / -20 °C

3: triethylamine / tetrahydrofuran / 0 - 20 °C

4: tetrahydrofuran / -40 °C / Inert atmosphere

With 1H-imidazole; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201203316

Reference yield:

: 133187-21-0
Methyl (S)-(+)-α-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-α-phenylacetate

: 1402909-66-3
C₂₆H₃₃OPSi

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / -20 °C

2: triethylamine / tetrahydrofuran / 0 - 20 °C

3: tetrahydrofuran / -40 °C / Inert atmosphere

With diisobutylaluminium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1002/anie.201203316

Reference yield:

: 17199-29-0
(S)-Mandelic acid

: 1402909-66-3
C₂₆H₃₃OPSi

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride

2: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C

3: diisobutylaluminium hydride / -20 °C

4: triethylamine / tetrahydrofuran / 0 - 20 °C

5: tetrahydrofuran / -40 °C / Inert atmosphere

With 1H-imidazole; thionyl chloride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201203316