C₁₅H₁₄Cl₂FN₅

Base Information

Chemical Name:C₁₅H₁₄Cl₂FN₅
CAS No.:1428640-40-7
Molecular Formula:C₁₅H₁₄Cl₂FN₅
Molecular Weight:354.214
Hs Code.:

C<sub>15</sub>H<sub>14</sub>Cl<sub>2</sub>FN<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₄Cl₂FN₅

Chemical Property:

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Technology Process of C₁₅H₁₄Cl₂FN₅

There total 11 articles about C₁₅H₁₄Cl₂FN₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428640-39-4
C₁₅H₁₅Cl₂N₅O

: 1428640-40-7
C₁₅H₁₄Cl₂FN₅

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane;
DOI:10.1021/jm4001314

Reference yield:

: 2401-21-0
1,2-Dichloro-3-iodobenzene

: 1428640-40-7
C₁₅H₁₄Cl₂FN₅

Guidance literature:: Multi-step reaction with 11 steps

1: copper / dimethyl sulfoxide

2: sodium hydroxide; water

3: oxalyl dichloride / N,N-dimethyl-formamide; hexane / 1 h / 20 °C

4: ammonia / water

5: trifluoroacetic anhydride

6: sodium hydride / tetrahydrofuran

7: hydrazine hydrate / ethanol

8: 8 h / 160 - 180 °C

9: potassium carbonate / N,N-dimethyl-formamide

10: sodium tetrahydroborate / methanol

11: diethylamino-sulfur trifluoride / dichloromethane

With sodium tetrahydroborate; oxalyl dichloride; diethylamino-sulfur trifluoride; ammonia; water; copper; sodium hydride; potassium carbonate; hydrazine hydrate; trifluoroacetic anhydride; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm4001314

Reference yield:

: C₈H₃Cl₃F₂O

: 1428640-40-7
C₁₅H₁₄Cl₂FN₅

Guidance literature:: Multi-step reaction with 8 steps

1: ammonia / water

2: trifluoroacetic anhydride

3: sodium hydride / tetrahydrofuran

4: hydrazine hydrate / ethanol

5: 8 h / 160 - 180 °C

6: potassium carbonate / N,N-dimethyl-formamide

7: sodium tetrahydroborate / methanol

8: diethylamino-sulfur trifluoride / dichloromethane

With sodium tetrahydroborate; diethylamino-sulfur trifluoride; ammonia; sodium hydride; potassium carbonate; hydrazine hydrate; trifluoroacetic anhydride; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm4001314