C₇H₁₁ClO

Base Information

Chemical Name:C₇H₁₁ClO
CAS No.:1583253-09-1
Molecular Formula:C₇H₁₁ClO
Molecular Weight:146.617
Hs Code.:

Synonyms:

Suppliers and Price of C₇H₁₁ClO

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(4R)-4-Chloro-6-Heptyn-1-ol
10mg
$ 1320.00

Total 2 raw suppliers

Chemical Property of C₇H₁₁ClO

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

(4R)-4-Chloro-6-Heptyn-1-ol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses (4R)-4-Chloro-6-heptyn-1-ol is a reactant used in the synthesis of Halichondrin compounds

Technology Process of C₇H₁₁ClO

There total 1 articles about C₇H₁₁ClO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1191268-97-9
C₂₃H₂₉ClOSi

: 1583253-09-1
C₇H₁₁ClO

Guidance literature:: With pyridine; pyridine hydrofluoride; In acetonitrile; at 0 - 20 ℃; for 10h;

Reference yield:

: 1583253-09-1
C₇H₁₁ClO

: 1583253-13-7
C₁₆H₁₉BrClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; dmap / dichloromethane / 5 h / 0 - 20 °C

2.1: B-Br-9-BBN / dichloromethane / 7 h / 0 °C

2.2: 0.83 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

4.1: dmap / dichloromethane / 1 h / 20 °C

With pyridine; B-Br-9-BBN; dmap; diisobutylaluminium hydride; In dichloromethane; toluene;
DOI:10.1021/ja5013307

Reference yield:

: 1583253-09-1
C₇H₁₁ClO

: 1583253-32-0
C₂₉H₃₄BrClO₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: pyridine; dmap / dichloromethane / 5 h / 0 - 20 °C

2.1: B-Br-9-BBN / dichloromethane / 7 h / 0 °C

2.2: 0.83 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

4.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1 h / 20 °C

5.1: C₁₄H₂₀N₂O₄S; chromium dichloride; zirconocene dichloride; lithium chloride; NiCl₂*2,9-dimethyl-1,10-phenanthroline complex; manganese / acetonitrile / 21 h / 20 °C / Glovebox

6.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1 h / 20 °C

7.1: pyridine hydrogenfluoride; pyridine / acetonitrile / 16 h / 20 °C

8.1: 3,3-dimethyldioxirane / acetone / 0.25 h / 0 °C

9.1: camphor-10-sulfonic acid / dichloromethane / 0.08 h / 20 °C

10.1: pyridine hydrogenfluoride / acetonitrile / 3 h / 20 °C

11.1: toluene-4-sulfonic acid / dichloromethane / 1 h / 20 °C

With pyridine; B-Br-9-BBN; chromium dichloride; dmap; manganese; zirconocene dichloride; C₁₄H₂₀N₂O₄S; camphor-10-sulfonic acid; NiCl₂*2,9-dimethyl-1,10-phenanthroline complex; 3,3-dimethyldioxirane; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; pyridine hydrogenfluoride; lithium chloride; In dichloromethane; acetone; toluene; acetonitrile;
DOI:10.1021/ja5013307