trans-2-(m-nitrophenyl)cyclopropanecarboxylic acid

Base Information

• Chemical Name: trans-2-(m-nitrophenyl)cyclopropanecarboxylic acid
• CAS No.: 84953-64-0
• Molecular Formula: C₁₀H₉NO₄
• Molecular Weight: 207.186

Synonyms:

Chemical Property of trans-2-(m-nitrophenyl)cyclopropanecarboxylic acid

Chemical Property:

Purity/Quality:

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Technology Process of trans-2-(m-nitrophenyl)cyclopropanecarboxylic acid

There total 7 articles about trans-2-(m-nitrophenyl)cyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(1RS,2RS)-ethyl 2-(3-nitrophenyl)cyclopropanecarboxylate → trans-2-(m-nitrophenyl)cyclopropanecarboxylic acid (84953-64-0,91880-89-6,115977-28-1,115977-30-5)

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃;

DOI:10.1016/j.ejmech.2015.02.060

Reference yield:

diazoacetic acid ethyl ester (623-73-4) + 1-nitro-3-vinyl-benzene (586-39-0,51209-60-0) → trans-2-(m-nitrophenyl)cyclopropanecarboxylic acid (84953-64-0,91880-89-6,115977-28-1,115977-30-5)

Guidance literature:

With xylene; at 140 ℃; Erhitzen des Reaktionsprodukts mit wss. Essigsaeure und H₂SO₄, Erwaermen des Saeuregemisches mit SOCl₂ in Benzol und anschliessende Hydrolyse mit H₂O;

DOI:10.1021/ja01548a051

Reference yield:

(1S,2S)-2-(3-Nitro-phenyl)-cyclopropanecarboxylic acid methyl ester → trans-2-(m-nitrophenyl)cyclopropanecarboxylic acid (84953-64-0,91880-89-6,115977-28-1,115977-30-5)

Guidance literature:

With sodium hydroxide; In methanol; water; at 20 ℃; for 2h;

DOI:10.1016/j.bmc.2004.02.037

upstream raw materials:

diazoacetic acid ethyl ester

1-nitro-3-vinyl-benzene

(E)-3-Nitrocinnamic acid

methyl 3-nitrocinnamate

Downstream raw materials:

trans-2-(3-chlorophenyl)-cyclopropanecarboxylic acid

(1R,2S)-2-(3-Nitro-phenyl)-cyclopropylamine

N⁶-[trans-2-(3-nitrophenyl)cyclopropyl]adenosine

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