ethyl 2-chloro-2-ethyl-3-phenylthiobutanoate

Base Information

Chemical Name:ethyl 2-chloro-2-ethyl-3-phenylthiobutanoate
CAS No.:108362-32-9
Molecular Formula:C₁₄H₁₉ClO₂S
Molecular Weight:286.823
Hs Code.:

Synonyms:

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Chemical Property of ethyl 2-chloro-2-ethyl-3-phenylthiobutanoate

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Technology Process of ethyl 2-chloro-2-ethyl-3-phenylthiobutanoate

There total 4 articles about ethyl 2-chloro-2-ethyl-3-phenylthiobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108362-27-2
ethyl 2-ethyl-3-oxo-2-phenylthiobutanoate

: 108362-32-9
ethyl 2-chloro-2-ethyl-3-phenylthiobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / zinc borohydride / diethyl ether / 4 h / Ambient temperature

2: SOCl₂, pyridine / CCl₄ / 0.08 h / 0 °C

With pyridine; thionyl chloride; zinc borohydride; In tetrachloromethane; diethyl ether;

Reference yield:

: 108-98-5
thiophenol

: 108362-32-9
ethyl 2-chloro-2-ethyl-3-phenylthiobutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydroxide, 3.) K₂CO₃ / 1.) ethanol, 2.) ethanol, 3.) acetone, reflux, 40 h

2: 96 percent / zinc borohydride / diethyl ether / 4 h / Ambient temperature

3: SOCl₂, pyridine / CCl₄ / 0.08 h / 0 °C

With pyridine; sodium hydroxide; thionyl chloride; zinc borohydride; potassium carbonate; In tetrachloromethane; diethyl ether;

Reference yield:

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 108362-32-9
ethyl 2-chloro-2-ethyl-3-phenylthiobutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydroxide, 3.) K₂CO₃ / 1.) ethanol, 2.) ethanol, 3.) acetone, reflux, 40 h

2: 96 percent / zinc borohydride / diethyl ether / 4 h / Ambient temperature

3: SOCl₂, pyridine / CCl₄ / 0.08 h / 0 °C

With pyridine; sodium hydroxide; thionyl chloride; zinc borohydride; potassium carbonate; In tetrachloromethane; diethyl ether;