Technology Process of trans-1,2-bis(benzoyloxy)-1,2,3,4-tetrahydrodibenz
anthracene
There total 8 articles about trans-1,2-bis(benzoyloxy)-1,2,3,4-tetrahydrodibenzanthracene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iodine;
In
tetrahydrofuran; benzene;
at 80 ℃;
for 3h;
DOI:10.1021/jo00342a041
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) hydrazine hydrate, 2.) KOH / 1.) triethylene glycol, 110 deg C, 60 min, 2.) 140 deg C, 2 h
2: 20 percent / benzene; acetic acid / 5 h / 80 °C
3: 99 percent / conc. HCl / acetic acid / 1 h / Heating
4: 66 percent / iodine / tetrahydrofuran; benzene / 3 h / 80 °C
With
potassium hydroxide; iodine; hydrazine hydrate;
hydrogenchloride;
In
tetrahydrofuran; acetic acid; benzene;
DOI:10.1021/jo00342a041
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 65 percent / n-pentanol, sodium / 4 h / Heating
2: 61 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / benzene / 96 h / Ambient temperature
3: 20 percent / benzene; acetic acid / 5 h / 80 °C
4: 99 percent / conc. HCl / acetic acid / 1 h / Heating
5: 66 percent / iodine / tetrahydrofuran; benzene / 3 h / 80 °C
With
pentan-1-ol; iodine; sodium; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
hydrogenchloride;
In
tetrahydrofuran; acetic acid; benzene;
DOI:10.1021/jo00342a041
