4-methylphenylsilyl chloride

Base Information

Chemical Name:4-methylphenylsilyl chloride
CAS No.:102368-04-7
Molecular Formula:C₁₉H₃₀ClNSi₃
Molecular Weight:392.163
Hs Code.:

4-<N,N-bis((trimethylsilyl)amino)phenyl>methylphenylsilyl chloride

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Suppliers and Price of 4-methylphenylsilyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methylphenylsilyl chloride

Chemical Property:

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Technology Process of 4-methylphenylsilyl chloride

There total 3 articles about 4-methylphenylsilyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-40-1
4-bromo-aniline

: 102368-04-7
4-methylphenylsilyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / triethylamine / tetrahydrofuran / 3 h / 45 °C

2: 1.) MeMgCl / 1.) 0 deg C, 2.) THF, 25 deg C

3: 1.) Mg, I₂ / 1.) THF, RT, 20 min, 2.) THF, RT, overnight

With iodine; methylmagnesium chloride; magnesium; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00363a006

Reference yield:

: 63911-87-5
N-(trimethylsilyl)-4-bromoaniline

: 102368-04-7
4-methylphenylsilyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MeMgCl / 1.) 0 deg C, 2.) THF, 25 deg C

2: 1.) Mg, I₂ / 1.) THF, RT, 20 min, 2.) THF, RT, overnight

With iodine; methylmagnesium chloride; magnesium;
DOI:10.1021/jo00363a006

Reference yield:

: 5089-33-8
2-(4-bromophenyl)-1,1,1,3,3,3-hexamethyldisilazane

: 149-74-6
dichloromethylphenylsilane

: 102368-04-7
4-methylphenylsilyl chloride

Guidance literature:: With iodine; magnesium; Yield given. Multistep reaction; 1.) THF, RT, 20 min, 2.) THF, RT, overnight;
DOI:10.1021/jo00363a006