Technology Process of (2S,3S)-4-azido-2,3-bis-benzyloxybutanoic acid
There total 4 articles about (2S,3S)-4-azido-2,3-bis-benzyloxybutanoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium dihydrogenphosphate; sodium hypochlorite solution; 2-methyl-but-2-ene;
In
tetrahydrofuran; water; tert-butyl alcohol;
at 20 ℃;
DOI:10.1021/cb5003416
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ozone; dimethylsulfide / dichloromethane
2: sodium hypochlorite solution; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 20 °C
With
sodium dihydrogenphosphate; sodium hypochlorite solution; 2-methyl-but-2-ene; dimethylsulfide; ozone;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/cb5003416
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide; ammonium chloride; methanol / water
2: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran
3: ozone; dimethylsulfide / dichloromethane
4: sodium hypochlorite solution; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 20 °C
With
methanol; sodium dihydrogenphosphate; sodium azide; sodium hypochlorite solution; 2-methyl-but-2-ene; dimethylsulfide; tetra-(n-butyl)ammonium iodide; sodium hydride; ammonium chloride; ozone;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/cb5003416
