Re₂(CO)8(CH₃CN)(C₆H₅CN)

Base Information

• Chemical Name: Re₂(CO)8(CH₃CN)(C₆H₅CN)
• CAS No.: 139576-00-4
• Molecular Formula: C₁₇H₈N₂O₈Re₂
• Molecular Weight: 740.673
• Mol file: 139576-00-4.mol

Synonyms:

Chemical Property of Re₂(CO)8(CH₃CN)(C₆H₅CN)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Re₂(CO)8(CH₃CN)(C₆H₅CN)

There total 1 articles about Re₂(CO)8(CH₃CN)(C₆H₅CN) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Re2(CO)9CH3CN (139406-04-5,67486-88-8) + benzonitrile (100-47-0) → Re2(CO)8(CH3CN)(C6H5CN) + Re2(CO)8(CH3CN)(C6H5CN) (139575-99-8,139576-00-4)

Guidance literature:

With trimethylamine-N-oxide; In acetonitrile; Re2(CO)9CH3CN, C6H5CN and 1.1 equiv. of Me3NO were reacted at 25°C; react. was monitored by IR, column chromy. on silica, eluent C6H14/ethyl acetate or C6H14/CH2Cl2, ratio of products 3.5:1;

DOI:10.1016/0022-328X(92)83023-B

upstream raw materials:

Re₂(CO)9CH₃CN

benzonitrile