(3aS,5S,6aR)-5-Benzenesulfinyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole

Base Information

Chemical Name:(3aS,5S,6aR)-5-Benzenesulfinyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole
CAS No.:110890-46-5
Molecular Formula:C₂₀H₂₂O₅S₂
Molecular Weight:406.524
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aS,5S,6aR)-5-Benzenesulfinyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole

Chemical Property:

Purity/Quality:

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Technology Process of (3aS,5S,6aR)-5-Benzenesulfinyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole

There total 4 articles about (3aS,5S,6aR)-5-Benzenesulfinyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110890-44-3
1-phenylthio-1-phenylsulfonyl-(3,4-isopropylidenedioxy)cyclopentane

: 110890-46-5
(3aS,5S,6aR)-5-Benzenesulfinyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole

Guidance literature:: With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 20h;

Reference yield:

: 15296-86-3
1-(phenylsulfanyl)methyl phenyl sulfone

: 110890-46-5
(3aS,5S,6aR)-5-Benzenesulfinyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / 50percent NaOH, (Bu)4NF / tetrahydrofuran; toluene / 2 h / Ambient temperature

2: sodium acetate, tetraethylammonium acetate, , TBHP, OsO₄ / acetone; H₂O / Ambient temperature

3: p-toluene sulfonic acid / CH₂Cl₂ / 1 h / Ambient temperature

4: K₂CO₃, MCPBA / CH₂Cl₂ / 20 h / 0 °C

With tert.-butylhydroperoxide; sodium hydroxide; osmium(VIII) oxide; tetrabutyl ammonium fluoride; tetraethylammonium acetate; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water; acetone; toluene;

Reference yield:

: 110890-38-5
1-phenylthio-1-phenylsulfonyl-3-cyclopentene

: 110890-46-5
(3aS,5S,6aR)-5-Benzenesulfinyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate, tetraethylammonium acetate, , TBHP, OsO₄ / acetone; H₂O / Ambient temperature

2: p-toluene sulfonic acid / CH₂Cl₂ / 1 h / Ambient temperature

3: K₂CO₃, MCPBA / CH₂Cl₂ / 20 h / 0 °C

With tert.-butylhydroperoxide; osmium(VIII) oxide; tetraethylammonium acetate; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; acetone;