Technology Process of C18H17N3O5S2
There total 11 articles about C18H17N3O5S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: Fe, 35percent HCl / ethanol; H2O / 0.25 h / Heating
3: 100 percent / methanol / Heating
4: 80 percent / KOH / dimethylformamide / 2 h / 80 °C
5: 98 percent / acide polyphosphorique (PPA) / 0.5 h / 120 °C
6: 95 percent / HCl / acetone / 0.5 h / Ambient temperature
7: 90 percent / methanol / Heating
8: aq. NaOH / methanol / Ambient temperature
With
hydrogenchloride; potassium hydroxide; sodium hydroxide; Acide polyphosphorique; iron;
In
methanol; ethanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0223-5234(91)90207-4
- Guidance literature:
-
Multi-step reaction with 11 steps
1: HNO3, H2SO4 / -10 °C
2: Na2Cr2O7, H2SO4
3: Cu / quinoline / 260 °C
4: Fe, 35percent HCl / ethanol; H2O / 0.25 h / Heating
6: 100 percent / methanol / Heating
7: 80 percent / KOH / dimethylformamide / 2 h / 80 °C
8: 98 percent / acide polyphosphorique (PPA) / 0.5 h / 120 °C
9: 95 percent / HCl / acetone / 0.5 h / Ambient temperature
10: 90 percent / methanol / Heating
11: aq. NaOH / methanol / Ambient temperature
With
hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium dichromate; Acide polyphosphorique; sulfuric acid; nitric acid; iron; copper;
In
quinoline; methanol; ethanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0223-5234(91)90207-4