(C₆H₅C(NOH)C(NO)C₆H₅)TiCl₃

Base Information

Chemical Name:(C₆H₅C(NOH)C(NO)C₆H₅)TiCl₃
CAS No.:21831-54-9
Molecular Formula:C₁₄H₁₁Cl₃N₂O₂Ti
Molecular Weight:393.493
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>C(NOH)C(NO)C<sub>6</sub>H<sub>5</sub>)TiCl<sub>3</sub>

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Chemical Property of (C₆H₅C(NOH)C(NO)C₆H₅)TiCl₃

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Technology Process of (C₆H₅C(NOH)C(NO)C₆H₅)TiCl₃

There total 1 articles about (C₆H₅C(NOH)C(NO)C₆H₅)TiCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 7550-45-0
titanium tetrachloride

: 23873-81-6
benzildioxime

: 356059-79-5,21831-54-9
(C₆H₅C(NOH)C(NO)C₆H₅)TiCl₃

Guidance literature:: With Na; i-PrOH; In isopropyl alcohol; benzene; byproducts: NaCl; under N2, 1 equiv. Na was dissolved in i-PrOH, stirring for 0.5 h at reflux temp., cooling, 1 equiv. of oxime was added, reflux for 2 h in 1:1 C6H6:i-PrOH mixt., 1 equiv. of TiCl4 was dropped at room temp., reflux for 2 h in dry benzene; NaCl was filtered off, solvent was removed. in vac., crystn. from C6H6-petroleum ether (40-60 °) (1:1, v/v), elem. anal.;
DOI:10.1081/SIM-100001940