Prⁱ₃Ge(GePh₂)₄GePrⁱ₃

Base Information

Chemical Name:Prⁱ₃Ge(GePh₂)₄GePrⁱ₃
CAS No.:1453070-91-1
Molecular Formula:C₆₆H₈₂Ge₆
Molecular Weight:1310.92
Hs Code.:

Pr<SUP>i</SUP><SUB>3</SUB>Ge(GePh<SUB>2</SUB>)<SUB>4</SUB>GePr<SUP>i</SUP><SUB>3</SUB>

Synonyms:

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Chemical Property of Prⁱ₃Ge(GePh₂)₄GePrⁱ₃

Chemical Property:

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Technology Process of Prⁱ₃Ge(GePh₂)₄GePrⁱ₃

There total 4 articles about Prⁱ₃Ge(GePh₂)₄GePrⁱ₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2117-71-7
octaphenylcyclotetragermane

: 1453070-91-1
Prⁱ₃Ge(GePh₂)₄GePrⁱ₃

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / benzene

2: lithium aluminium tetrahydride / diethyl ether / 18 h / 20 °C / Inert atmosphere

3: acetonitrile / 72 h / 90 °C / Schlenk technique

With lithium aluminium tetrahydride; bromine; In diethyl ether; acetonitrile; benzene;
DOI:10.1039/c3cc45450a

Reference yield:

: 37044-16-9
tetraphenyldigermanium dichloride

: 1453070-91-1
Prⁱ₃Ge(GePh₂)₄GePrⁱ₃

Guidance literature:: Multi-step reaction with 5 steps

1: benzene / 18 h / Inert atmosphere

2: acetonitrile / 48 h / 85 °C / Inert atmosphere; Sealed tube; Schlenk technique

3: benzene / Inert atmosphere

4: diethyl ether / 18 h / 20 °C / Inert atmosphere

5: acetonitrile / 72 h / 90 °C / Inert atmosphere; Sealed tube; Schlenk technique

In diethyl ether; acetonitrile; benzene;
DOI:10.1139/cjc-2013-0485

Reference yield:

: Me₂NPh₂GeGePh₂NMe₂

: 1453070-91-1
Prⁱ₃Ge(GePh₂)₄GePrⁱ₃

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 48 h / 85 °C / Inert atmosphere; Sealed tube; Schlenk technique

2: benzene / Inert atmosphere

3: diethyl ether / 18 h / 20 °C / Inert atmosphere

4: acetonitrile / 72 h / 90 °C / Inert atmosphere; Sealed tube; Schlenk technique

In diethyl ether; acetonitrile; benzene;
DOI:10.1139/cjc-2013-0485