1,1,2,2-Tetraphenyl-1,2-dichlorodigermane

Base Information

Chemical Name:1,1,2,2-Tetraphenyl-1,2-dichlorodigermane
CAS No.:37044-16-9
Molecular Formula:C24H20Cl2Ge2
Molecular Weight:524.509
Hs Code.:
NSC Number:361596
Nikkaji Number:J3.371.041K

Synonyms:37044-16-9;NSC361596;NSC-361596;1,1,2,2-Tetraphenyl-1,2-dichlorodigermane

Suppliers and Price of 1,1,2,2-Tetraphenyl-1,2-dichlorodigermane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,1,2,2-Tetraphenyl-1,2-dichlorodigermane

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:523.937460
Heavy Atom Count:28
Complexity:321

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Ge](C2=CC=CC=C2)Cl.C1=CC=C(C=C1)[Ge](C2=CC=CC=C2)Cl

Technology Process of 1,1,2,2-Tetraphenyl-1,2-dichlorodigermane

There total 7 articles about 1,1,2,2-Tetraphenyl-1,2-dichlorodigermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 68261-58-5
((C₆H₅)2ClGe)2Hg

: 37044-16-9
tetraphenyldigermanium dichloride

Guidance literature:: In benzene; byproducts: Hg; refluxed with stirring for 1 h; evapn., recrystn. (toluene/pentane);
DOI:10.1016/S0022-328X(00)85661-2

Reference yield: 87.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 2816-39-9
hexaphenyldigermane

: 37044-16-9
tetraphenyldigermanium dichloride

: 112174-88-6
1,1,2-trichlorotriphenyldigermane

Guidance literature:: In neat (no solvent); High Pressure; pressure react. of dry HCl and Ph6Ge2 in autoclave (molar ratio HCl/Ph6Ge2 = 7.3), room temp., initial pressure 34 atm, 24h; rinsing react. mixt. with pentane into retort; evapn.; addn. of pentane; cooling to -15°C; crystn. overnight; filtration; recrystn. (petroleum ether); elem. anal.;

Reference yield: 77.0%

: 91986-03-7
1,2-bis(trichloroacetate)tetraphenyldigermane

: 37044-16-9
tetraphenyldigermanium dichloride

Guidance literature:: With HCl; In acetone; byproducts: CCl3COOH; heated at 50°C for 12 h; cooled at -30°C;; washing with acetone/n-hexane; recrystn. twice from ether/cyclohexane;;
DOI:10.1016/0022-328X(84)80168-0