Germane, diiodobis(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:Germane, diiodobis(2,4,6-trimethylphenyl)-
CAS No.:106092-58-4
Molecular Formula:C18H22GeI2
Molecular Weight:564.772
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germane, diiodobis(2,4,6-trimethylphenyl)-

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Technology Process of Germane, diiodobis(2,4,6-trimethylphenyl)-

There total 1 articles about Germane, diiodobis(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106092-68-6
dimesityldimethoxygermane

: 106092-58-4
dimesityldiiodogermane

Guidance literature:: With hydrogen iodide; In water; benzene; addn. of a soln. of acid in H2O to a soln. of germane in benzene (N2), stirring for 2 h at 60°C; extn. with pentane, drying over Na2SO4, evapn. (reduced pressure), recrystn. in pentane; elem. anal.;
DOI:10.1021/ja00236a016

Reference yield: 70.0%

: 106092-58-4
dimesityldiiodogermane

: 83115-13-3
lithium 2,4,6-tris(tert-butyl)phenylphosphide

: 106092-59-5
((CH₃)3C₆H₂)2GeIP(H)C₆H₂(C(CH₃)3)3

Guidance literature:: In diethyl ether; hexane; pentane; slow addn. of a soln. of lithiophosphide (prepd. from 2,4,6-tri-tert-butylphenylphosphine, butyllithium in hexane and diethyl ether) to a soln. of germane in pentane, 1 h at room temp. (N2); evapn. (reduced pressure), recrystn. from pentane;
DOI:10.1021/ja00236a016