Germane, dimethoxybis(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:Germane, dimethoxybis(2,4,6-trimethylphenyl)-
CAS No.:106092-68-6
Molecular Formula:C20H28GeO2
Molecular Weight:373.031
Hs Code.:

Synonyms:

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Chemical Property of Germane, dimethoxybis(2,4,6-trimethylphenyl)-

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Technology Process of Germane, dimethoxybis(2,4,6-trimethylphenyl)-

There total 2 articles about Germane, dimethoxybis(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 96481-42-4
dichlorodimesitylgermane

: 106092-68-6
dimesityldimethoxygermane

Guidance literature:: With methanol; triethylamine; In benzene; byproducts: HCl; (Ar or N2), dry solvents; addn. of MeOH and excess of Et3N to a soln. of the Ge-compd. in benzene, standing in a Schlenk tube at 40°C (3 h);; concn. (reduced pressure), filtration, concn. of filtrate (0.01 mm Hg), recrystn. in the cold (C6H6); elem. anal.;;

Reference yield:

: 67-56-1
methanol

: 143367-75-3
N-dimesitylfluorogermyl-N-tri-t-butyl-2,4,6-phenylamine

: 106092-68-6
dimesityldimethoxygermane

Guidance literature:: In benzene-d6; addn. of CH3OH to soln. of (C6H2(CH3)3)2Ge(F)N(H)C6H2(C(CH3)3)3 (0.033 mmol) in C6D6 at 20°C (1 wk);; formation of 25% (C6H2(CH3)3)2Ge(OCH3)2, detected by 19F- and 1H-NMR;;

Reference yield: 96.0%

: 106092-68-6
dimesityldimethoxygermane

: 96481-36-6
dimesityldifluorogermane

Guidance literature:: With hydrogen fluoride; In tetrahydrofuran; byproducts: methanol; (Ar or N2), dry solvents; addn. of excess of HF (40%) to a soln. of the Ge-compd. in THF, stirring at 30°C (30 min);; extn. (benzene), drying (Na2SO4, 12 h), concn. (reduced pressure), redissolving (THF), drying (Na2SO4, 2 h), concn. (reduced pressure), crystn. (benzene); elem. anal.;;