4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate]

Base Information

Chemical Name:4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate]
CAS No.:1616956-91-2
Molecular Formula:C₆₃H₈₀O₁₀
Molecular Weight:997.322
Hs Code.:

Synonyms:

Suppliers and Price of 4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate]

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate]

There total 6 articles about 4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616956-74-1
4-(4-n-tetradecylphenoxycarbonyl)benzaldehyde

: 1616956-91-2
4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate]

Guidance literature:: Multi-step reaction with 3 steps

1: recorcinol; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 20 °C

2: thionyl chloride; N,N-dimethyl-formamide / 1 h / Reflux

3: triethylamine; pyridine / dichloromethane / 6 h / Inert atmosphere; Reflux

With pyridine; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; triethylamine; N,N-dimethyl-formamide; recorcinol; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c4tc00533c

Reference yield:

: 1616956-75-2
4-(4-n-tetradecylphenoxycarbonyl)benzoic acid

: 1616956-91-2
4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate]

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / 1 h / Reflux

2: triethylamine; pyridine / dichloromethane / 6 h / Inert atmosphere; Reflux

With pyridine; thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c4tc00533c

Reference yield:

: 25401-89-2
4-n-tetradecylphenol

: 1616956-91-2
4-methyl-1,3-phenylene bis-[4-(4-n-tetradecyloxyphenoxy)carbonyl benzoate]

Guidance literature:: Multi-step reaction with 4 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 24 h

2: recorcinol; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 20 °C

3: thionyl chloride; N,N-dimethyl-formamide / 1 h / Reflux

4: triethylamine; pyridine / dichloromethane / 6 h / Inert atmosphere; Reflux

With pyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; triethylamine; N,N-dimethyl-formamide; dicyclohexyl-carbodiimide; recorcinol; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c4tc00533c