C₁₇H₁₂F₃N₃

Base Information

Chemical Name:C₁₇H₁₂F₃N₃
CAS No.:1279722-79-0
Molecular Formula:C₁₇H₁₂F₃N₃
Molecular Weight:315.298
Hs Code.:

C<sub>17</sub>H<sub>12</sub>F<sub>3</sub>N<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₂F₃N₃

Chemical Property:

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Technology Process of C₁₇H₁₂F₃N₃

There total 3 articles about C₁₇H₁₂F₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1279722-81-4
Br^(1-)*C₂₈H₂₃F₃P⁽¹⁺⁾

: 16714-25-3
2-azidobenzaldehyde

: C₁₇H₁₂F₃N₃

: 1279722-79-0
C₁₇H₁₂F₃N₃

Guidance literature:: Br^(1-)*C₂₈H₂₃F₃P⁽¹⁺⁾; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

2-azidobenzaldehyde; In tetrahydrofuran; hexane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201006917

Reference yield:

: C₁₀H₈BrF₃

: C₁₇H₁₂F₃N₃

: 1279722-79-0
C₁₇H₁₂F₃N₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 16 h / Inert atmosphere; Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; toluene; 2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1002/anie.201006917

Reference yield:

: 150969-56-5
5-(trifluoromethyl)-2,3-dihydro-1H-inden-1-one

: C₁₇H₁₂F₃N₃

: 1279722-79-0
C₁₇H₁₂F₃N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / ethanol / Inert atmosphere

2.1: hydrogen bromide / dichloromethane; water

3.1: toluene / 16 h / Inert atmosphere; Reflux

4.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 20 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; hydrogen bromide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene; 4.1: Wittig reaction / 4.2: Wittig reaction;
DOI:10.1002/anie.201006917