C₁₆H₁₅NO₆

Base Information

• Chemical Name: C₁₆H₁₅NO₆
• CAS No.: 1438020-55-3
• Molecular Formula: C₁₆H₁₅NO₆
• Molecular Weight: 317.298
• Mol file: 1438020-55-3.mol

Synonyms:

Chemical Property of C₁₆H₁₅NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₅NO₆

There total 1 articles about C₁₆H₁₅NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

C16H17NO4 (1438020-52-0) → C16H15NO6 (1438020-55-3)

Guidance literature:

C₁₆H₁₇NO₄; With sulfuryl dichloride; bromine; acetic acid; at 10 - 20 ℃; for 5h;

With water; at 20 ℃; for 1h; regioselective reaction;

DOI:10.1021/ja4025148

Reference yield: 63.0%

C16H15NO6 (1438020-55-3) + tert-butyl alcohol (75-65-0) → C20H23NO6 (1438020-58-6)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 12h;

DOI:10.1021/ja4025148

Reference yield:

C16H15NO6 (1438020-55-3) → C25H34N2O5 (1438020-76-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h

2.1: palladium 10% on activated carbon; formic acid; hydrogen / methanol / 2 h

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 70 °C

3.2: 12 h / 20 °C

With dmap; formic acid; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja4025148

upstream raw materials:

C₁₆H₁₇NO₄

Downstream raw materials:

C₂₀H₂₃NO₆

C₂₅H₃₄N₂O₅

C₂₁H₂₆N₂O₅

C₂₇H₃₇N₅O₆