3-Ethyliden-1,1-diphenylcyclobutan

Base Information

• Chemical Name: 3-Ethyliden-1,1-diphenylcyclobutan
• CAS No.: 122408-65-5
• Molecular Formula: C₁₈H₁₈
• Molecular Weight: 234.341
• Mol file: 122408-65-5.mol

Synonyms:

Chemical Property of 3-Ethyliden-1,1-diphenylcyclobutan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Ethyliden-1,1-diphenylcyclobutan

There total 2 articles about 3-Ethyliden-1,1-diphenylcyclobutan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

3,3-diphenylcyclobutanone (54166-20-0) + ethylenetriphenylphosphorane (1754-88-7) → 3-Ethyliden-1,1-diphenylcyclobutan (122408-65-5)

Guidance literature:

In diethyl ether; for 0.5h; Heating;

Reference yield:

2,2-dichloro-3,3-diphenylcyclobutanone (122408-62-2) → 3-Ethyliden-1,1-diphenylcyclobutan (122408-65-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / zinc powder / acetic acid / 48 h / Ambient temperature

2: 68 percent / diethyl ether / 0.5 h / Heating

With zinc; In diethyl ether; acetic acid;

upstream raw materials:

3,3-diphenylcyclobutanone

ethylenetriphenylphosphorane

2,2-dichloro-3,3-diphenylcyclobutanone

Refernces