2,2-dichloro-3,3-diphenylcyclobutanone

Base Information

Chemical Name:2,2-dichloro-3,3-diphenylcyclobutanone
CAS No.:122408-62-2
Molecular Formula:C₁₆H₁₂Cl₂O
Molecular Weight:291.177
Hs Code.:

Synonyms:2,2-dichloro-3,3-diphenylcyclobutanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-dichloro-3,3-diphenylcyclobutanone

Chemical Property:

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Technology Process of 2,2-dichloro-3,3-diphenylcyclobutanone

There total 5 articles about 2,2-dichloro-3,3-diphenylcyclobutanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 530-48-3
1,1-Diphenylethylene

: 76-02-8
trifluoroacetyl chloride

: 122408-62-2
2,2-dichloro-3,3-diphenylcyclobutanone

Guidance literature:: With zinc; trichlorophosphate;
DOI:10.1021/ja0602501

Reference yield:

: 119-61-9
benzophenone

: 122408-62-2
2,2-dichloro-3,3-diphenylcyclobutanone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

2: zinc-copper couple; trichlorophosphate / diethyl ether / 20 °C / Inert atmosphere; Schlenk technique

With zinc-copper couple; potassium tert-butylate; trichlorophosphate; In tetrahydrofuran; diethyl ether; 1: |Wittig Olefination;
DOI:10.1039/c5cc01415h

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 122408-62-2
2,2-dichloro-3,3-diphenylcyclobutanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: trichlorophosphate; zinc/copper couple / diethyl ether / Inert atmosphere; Reflux

With zinc/copper couple; trichlorophosphate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/acs.orglett.1c03938