1-(3'-[chloro(triphenylphosphine)platino]-4'-[(dimethylamino)methyl]benzyl)-3-ethylmalonate

Base Information

Chemical Name:1-(3'-[chloro(triphenylphosphine)platino]-4'-[(dimethylamino)methyl]benzyl)-3-ethylmalonate
CAS No.:399042-66-1
Molecular Formula:C₃₃H₃₅ClNO₄PPt
Molecular Weight:771.152
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3'-[chloro(triphenylphosphine)platino]-4'-[(dimethylamino)methyl]benzyl)-3-ethylmalonate

Chemical Property:

Purity/Quality:

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Technology Process of 1-(3'-[chloro(triphenylphosphine)platino]-4'-[(dimethylamino)methyl]benzyl)-3-ethylmalonate

There total 3 articles about 1-(3'-[chloro(triphenylphosphine)platino]-4'-[(dimethylamino)methyl]benzyl)-3-ethylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 399042-59-2
3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl alcohol

: 36239-09-5
ethyl chlorocarbonylacetate

: 399042-66-1
1-(3'-[chloro(triphenylphosphine)platino]-4'-[(dimethylamino)methyl]benzyl)-3-ethylmalonate

Guidance literature:: With triethyl amine; In dichloromethane; to a soln. of complex in CH2Cl2 at 0°C was added (C2H5)3N and ethyl malonyl chloride, the mixt. was stirred for 5 h (N2); evapd. in vac., the solid was washed with diethyl ether, dissolved in CH2Cl2, washed with satd. soln. of NaHCO3, and satd. soln. of NaCl, dried on MgSO4, evapd. in vac.; elem. anal.;
DOI:10.1021/om010500g

Reference yield:

: 3-[chloro(dimethylsulfoxide)platino]-4-[(dimethylamino)methyl]benzyl alcohol

: 399042-66-1
1-(3'-[chloro(triphenylphosphine)platino]-4'-[(dimethylamino)methyl]benzyl)-3-ethylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: triethyl amine / dichloromethane

With triethyl amine; In dichloromethane;
DOI:10.1021/om010500g

Reference yield:

: 603-35-0
triphenylphosphine

: 399042-66-1
1-(3'-[chloro(triphenylphosphine)platino]-4'-[(dimethylamino)methyl]benzyl)-3-ethylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: triethyl amine / dichloromethane

With triethyl amine; In dichloromethane;
DOI:10.1021/om010500g