AlMeCl(2-(2,6-iPr₂C₆H₃NCH)-5-tBuC₄H₂N)

Base Information

• Chemical Name: AlMeCl(2-(2,6-iPr₂C₆H₃NCH)-5-tBuC₄H₂N)
• CAS No.: 1361927-47-0
• Molecular Formula: C₂₂H₃₂AlClN₂
• Molecular Weight: 386.944

Synonyms:

Chemical Property of AlMeCl(2-(2,6-iPr₂C₆H₃NCH)-5-tBuC₄H₂N)

Chemical Property:

Purity/Quality:

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Technology Process of AlMeCl(2-(2,6-iPr₂C₆H₃NCH)-5-tBuC₄H₂N)

There total 3 articles about AlMeCl(2-(2,6-iPr₂C₆H₃NCH)-5-tBuC₄H₂N) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N-(2,6-bis(isopropyl)phenyl)-5-tert-butylpyrrolylaldimine (443890-22-0) + methylaluminum dichloride (917-65-7) → AlMeCl(2-(2,6-iPr2C6H3NCH)-5-tBuC4H2N) (1361927-47-0)

Guidance literature:

In toluene; (under N2 or Ar); mixt. of AlCH3Cl2 and ligand in toluene refluxed for 2h; volatiles removed under vac., extd. with n-hexane, concd.; elem. anal.;

DOI:10.1021/om201252k

Reference yield:

(2-(2,6-iPr2C6H3NCH)-5-tBuC4H2N)*AlMe2Cl → AlMeCl(2-(2,6-iPr2C6H3NCH)-5-tBuC4H2N) (1361927-47-0)

Guidance literature:

In toluene; Al-complex in toluene degraded at elevated temp.;

DOI:10.1021/om201252k

Reference yield:

Li(2-(2,6-iPr2C6H3NCH)-5-tBuC4H2N) + dimethylaluminum chloride (1184-58-3) → AlMeCl(2-(2,6-iPr2C6H3NCH)-5-tBuC4H2N) (1361927-47-0)

Guidance literature:

In toluene; (under N2 or Ar); Al(CH3)2Cl and ligand in toluene refluxed for 2 h;

DOI:10.1021/om201252k

upstream raw materials:

dimethylaluminum chloride

N-(2,6-bis(isopropyl)phenyl)-5-tert-butylpyrrolylaldimine

methylaluminum dichloride

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