N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester>-pterin

Base Information

Chemical Name:N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester>-pterin
CAS No.:171777-71-2
Molecular Formula:C₂₅H₂₉N₇O₇
Molecular Weight:543.516
Hs Code.:

N(2')-acetyl-6-<N-(4-amino<2,3,5,6-2H4>benzoyl)-L-glutamic acid diethyl ester>-pterin

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Chemical Property of N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester>-pterin

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Technology Process of N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester>-pterin

There total 8 articles about N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester>-pterin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 171777-70-1
N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin

: 171777-71-2
N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester>-pterin

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 45 ℃;
DOI:10.1002/jlcr.2580361010

Reference yield:

: 2037-26-5
⁽²⁾H₈-toluene

: 171777-71-2
N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester>-pterin

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) HNO₃, <2H₂>sulfuric acid, 2.) sodium dichromate, H₂SO₄ / 1.) D₂O, 1.5 h, 2.) H₂O, reflux, 5 h

2: 2.43 g / PCl₅ / 0.25 h / 60 °C

3: 2.39 g / triethylamine / benzene / 0.25 h / Ambient temperature

4: 0.862 g / H₂ / 10percent Pd/C / ethanol / 1 h

5: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr

6: 118 mg / sodium borohydride / ethanol / 45 °C

With sodium tetrahydroborate; sodium dichromate; phosphorus pentachloride; sulfuric acid; hydrogen; nitric acid; sulfuric acid-d2; triethylamine; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1002/jlcr.2580361010

Reference yield:

: 171777-66-5
4-nitro<2,3,5,6-2H4>benzoic acid

: 171777-71-2
N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester>-pterin

Guidance literature:: Multi-step reaction with 5 steps

1: 2.43 g / PCl₅ / 0.25 h / 60 °C

2: 2.39 g / triethylamine / benzene / 0.25 h / Ambient temperature

3: 0.862 g / H₂ / 10percent Pd/C / ethanol / 1 h

4: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr

5: 118 mg / sodium borohydride / ethanol / 45 °C

With sodium tetrahydroborate; phosphorus pentachloride; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1002/jlcr.2580361010