1,2-di(α-thienyl)-1,2-ethanediol

Base Information

Chemical Name:1,2-di(α-thienyl)-1,2-ethanediol
CAS No.:51578-64-4
Molecular Formula:C₁₀H₁₀O₂S₂
Molecular Weight:226.32
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-di(α-thienyl)-1,2-ethanediol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 1,2-di(α-thienyl)-1,2-ethanediol

There total 3 articles about 1,2-di(α-thienyl)-1,2-ethanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 98-03-3
thiophene-2-carbaldehyde

: 1521-51-3,113667-32-6
rac-3-bromocyclohexene

: 51578-64-4
1,2-di(α-thienyl)-1,2-ethanediol

: C₁₁H₁₄OS

Guidance literature:: With lithium tetrafluoroborate; 3,7-di([1,1′-biphenyl]-4-yl)-10-(naphthalen-1-yl)-10H-phenoxazine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl acetamide; at 25 ℃; for 3h; Inert atmosphere; UV-irradiation;
DOI:10.1039/C8SC02038H

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 1204-86-0
4-(4-morpholinyl)benzaldehyde

: 51578-64-4
1,2-di(α-thienyl)-1,2-ethanediol

: erythro-1-(4-morpholinophenyl)-2-(thiophen-2-yl)ethane-1,2-diol

: threo-1-(4-morpholinophenyl)-2-(thiophen-2-yl)ethane-1,2-diol

: 1143504-65-7
C₂₂H₂₈N₂O₄

Guidance literature:: With manganese; titanium tetrachloride; In tetrahydrofuran; at -10 ℃; for 0.666667h; optical yield given as %de; Inert atmosphere;
DOI:10.1055/s-0028-1083264

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 18266-94-9
(Z)-1,2-bis(thiophene-2-yl)ethene

: 51578-64-4
1,2-di(α-thienyl)-1,2-ethanediol

: 13640-78-3
(E)-1,2-bis(2-thienyl)ethene

Guidance literature:: With chloro-trimethyl-silane; titanium(IV)isopropoxide; magnesium; triethylamine; In tetrahydrofuran; at 40 ℃; for 72h; optical yield given as %de;
DOI:10.1016/j.tetlet.2009.11.027