1D-2,3,6-Tri-O-benzyl-myo-inositol 1,4,5-tris

Base Information

Chemical Name:1D-2,3,6-Tri-O-benzyl-myo-inositol 1,4,5-tris
CAS No.:145842-34-8
Molecular Formula:C₄₅H₅₁N₆O₁₅P₃
Molecular Weight:1008.85
Hs Code.:

1D-2,3,6-Tri-O-benzyl-myo-inositol 1,4,5-tris<di-(2-cyanoethyl) phosphate>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-2,3,6-Tri-O-benzyl-myo-inositol 1,4,5-tris

Chemical Property:

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Technology Process of 1D-2,3,6-Tri-O-benzyl-myo-inositol 1,4,5-tris

There total 29 articles about 1D-2,3,6-Tri-O-benzyl-myo-inositol 1,4,5-tris which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 109522-11-4,145842-33-7
Phosphorous acid bis-(2-cyano-ethyl) ester (1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester

: 109522-12-5,112294-74-3,141040-51-9,145842-34-8,145842-35-9,147127-66-0
Phosphoric acid bis-(2-cyano-ethyl) ester (1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-[bis-(2-cyano-ethoxy)-phosphoryloxy]-cyclohexyl ester

Guidance literature:: With tert.-butylhydroperoxide;
DOI:10.1016/S0040-4039(00)96110-0

Reference yield:

: 100-39-0
benzyl bromide

: 145842-34-8
1D-2,3,6-Tri-O-benzyl-myo-inositol 1,4,5-tris

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / sodium hydride / dimethylformamide / 16 h / 20 °C

2: Huenig's base / [(Ph₃P)3RhCl] / ethanol; H₂O; toluene / 2 h / Heating

3: 117 mg / acetyl chloride / methanol; CH₂Cl₂ / 1.17 h / 20 °C

4: 1H-tetrazole / CH₂Cl₂ / 45 h

5: 291 mg / mCPBA / CH₂Cl₂ / -78 - 20 °C

With 1H-tetrazole; sodium hydride; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; Wilkinson's catalyst; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1071/CH06357

Reference yield:

: 104873-74-7
1D-1,4,5-tri-O-allyl-3,6-di-O-benzyl-myo-inositol

: 145842-34-8
1D-2,3,6-Tri-O-benzyl-myo-inositol 1,4,5-tris

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / sodium hydride / dimethylformamide / 16 h / 20 °C

2: Huenig's base / [(Ph₃P)3RhCl] / ethanol; H₂O; toluene / 2 h / Heating

3: 117 mg / acetyl chloride / methanol; CH₂Cl₂ / 1.17 h / 20 °C

4: 1H-tetrazole / CH₂Cl₂ / 45 h

5: 291 mg / mCPBA / CH₂Cl₂ / -78 - 20 °C

With 1H-tetrazole; sodium hydride; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; Wilkinson's catalyst; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1071/CH06357