2-[(4-Nitrophenyl)methyl]-2-phenyl-1,3-dioxolane

Base Information

Chemical Name:2-[(4-Nitrophenyl)methyl]-2-phenyl-1,3-dioxolane
CAS No.:106111-25-5
Molecular Formula:C16H15NO4
Molecular Weight:285.299
Hs Code.:
DSSTox Substance ID:DTXSID80555629
Nikkaji Number:J3.229.534G
Wikidata:Q82437028

Synonyms:106111-25-5;2-[(4-Nitrophenyl)methyl]-2-phenyl-1,3-dioxolane;DTXSID80555629

Suppliers and Price of 2-[(4-Nitrophenyl)methyl]-2-phenyl-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 2-[(4-Nitrophenyl)methyl]-2-phenyl-1,3-dioxolane

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:285.10010796
Heavy Atom Count:21
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC(O1)(CC2=CC=C(C=C2)[N+](=O)[O-])C3=CC=CC=C3

Technology Process of 2-[(4-Nitrophenyl)methyl]-2-phenyl-1,3-dioxolane

There total 4 articles about 2-[(4-Nitrophenyl)methyl]-2-phenyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 107-21-1
ethylene glycol

: 3769-82-2
2-(4-nitrophenyl)-1-phenylethanone

: 106111-25-5
α-(p-nitrophenyl)acetophenone ethylene glycol ketal

Guidance literature:: sulfuric acid; In toluene; for 3h; Heating;
DOI:10.1021/ja00221a038

Reference yield:

: 104-03-0
4-nitrobenzeneacetic acid

: 106111-25-5
α-(p-nitrophenyl)acetophenone ethylene glycol ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) thionyl chloride; 2.) AlCl₃ / 1.) ca. 55 deg C, 20 min; 2.) refl., 45 min

2: 87 percent / conc.H₂SO₄ / toluene / 3 h / Heating

With aluminium trichloride; thionyl chloride; sulfuric acid; In toluene;
DOI:10.1021/ja00221a038

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 106111-25-5
α-(p-nitrophenyl)acetophenone ethylene glycol ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) thionyl chloride; 2.) AlCl₃ / 1.) ca. 55 deg C, 20 min; 2.) refl., 45 min

2: 87 percent / conc.H₂SO₄ / toluene / 3 h / Heating

With aluminium trichloride; thionyl chloride; sulfuric acid; In toluene;
DOI:10.1021/ja00221a038