4-ferrocenyl-1-(4-benzyloxyphenyl)-1H-1,2,3-triazole

Base Information

Chemical Name:4-ferrocenyl-1-(4-benzyloxyphenyl)-1H-1,2,3-triazole
CAS No.:1391092-32-2
Molecular Formula:C₂₅H₂₁FeN₃O
Molecular Weight:435.308
Hs Code.:

Synonyms:

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Chemical Property of 4-ferrocenyl-1-(4-benzyloxyphenyl)-1H-1,2,3-triazole

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Technology Process of 4-ferrocenyl-1-(4-benzyloxyphenyl)-1H-1,2,3-triazole

There total 1 articles about 4-ferrocenyl-1-(4-benzyloxyphenyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 94040-95-6
1-azido-4-(benzyloxy)benzene

: 1-azidoferrocene

: 1391092-32-2
4-ferrocenyl-1-(4-benzyloxyphenyl)-1H-1,2,3-triazole

Guidance literature:: With CuSO₄; sodium ascorbate; tris((1-tert-butyl)-1H-1,2,3-triazol-4-yl)amine; In methanol; water; Schlenk technique; mixt. of CuSO4, sodium ascorbate and amine added to soln. of azide, stirred at room temp. for 72 h; water added, extd. with ethyl acetate, organic layer washed (water, brine), dried (Na2SO4), chromy. (silica gel, CHCl3 - ethyl acetate(0-25%)); elem. anal.;
DOI:10.1016/j.jorganchem.2012.05.042

Reference yield: 81.0%

: 6793-92-6
p-benzyloxyphenylbromide

: 1391092-32-2
4-ferrocenyl-1-(4-benzyloxyphenyl)-1H-1,2,3-triazole

: 1391092-35-5
4-ferrocenyl-1,5-bis(4-benzyloxyphenyl)-1H-1,2,3-triazole

Guidance literature:: With N(C₄H₉)4CH₃COO; Pd(P(C₆H₅)4)Cl₂; In further solvent(s); Schlenk technique; Fe-complex, N(C4H9)4CH3CO2 and benzene derivative placed into Schlenk tube, 1-methyl-2-pyrrolidinone and Pd-complex added, tube placed in oil bath heated to 100 °C, mixt. stirred at 100 °C for 2 h; solvent removed to dryness, chromy. (silica gel, CHCl3); elem. anal.;
DOI:10.1016/j.jorganchem.2012.05.042