-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester

Base Information

Chemical Name:-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester
CAS No.:212832-85-4
Molecular Formula:C₂₀H₂₁NO₄
Molecular Weight:339.391
Hs Code.:

<S-(E)>-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester

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Chemical Property of -2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester

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Technology Process of -2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester

There total 3 articles about -2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 212832-73-0
-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 212832-85-4
-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester

Guidance literature:: In methanol; hexane; benzene;
DOI:10.1248/cpb.46.1094

Reference yield:

: 615-37-2
ortho-methylphenyl iodide

: 212832-85-4
-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / aq. NaHCO₃, Pd(OAc)2, Bu₄NCl / 24 h / 45 °C

2: 60 percent / hexane; methanol; benzene

With palladium diacetate; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; In methanol; hexane; benzene;
DOI:10.1248/cpb.46.1094

Reference yield:

: 75266-42-1
(S)-2-<(benzyloxycarbonyl)amino>-3-butenoic acid

: 212832-85-4
-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / aq. NaHCO₃, Pd(OAc)2, Bu₄NCl / 24 h / 45 °C

2: 60 percent / hexane; methanol; benzene

With palladium diacetate; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; In methanol; hexane; benzene;
DOI:10.1248/cpb.46.1094