1-(4-{[(1E)-2-(4-acetylphenyl)-2,3-dihydro-1H-isoindol-1-ylidene]amino}phenyl)ethanone

Base Information

• Chemical Name: 1-(4-{[(1E)-2-(4-acetylphenyl)-2,3-dihydro-1H-isoindol-1-ylidene]amino}phenyl)ethanone
• CAS No.: 60025-39-0
• Molecular Formula: C24H20 N2 O2
• Molecular Weight: 368.4278

Synonyms:1-(p-Acetophenylimino)-2-(p-acetophenyl)isoindoline;NSC 335773

Chemical Property of 1-(4-{[(1E)-2-(4-acetylphenyl)-2,3-dihydro-1H-isoindol-1-ylidene]amino}phenyl)ethanone

Chemical Property:

• Vapor Pressure: 2.2E-13mmHg at 25°C
• Boiling Point: 578.6°Cat760mmHg
• Flash Point: 303.7°C
• Density: 1.17g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

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Technology Process of 1-(4-{[(1E)-2-(4-acetylphenyl)-2,3-dihydro-1H-isoindol-1-ylidene]amino}phenyl)ethanone

There total 3 articles about 1-(4-{[(1E)-2-(4-acetylphenyl)-2,3-dihydro-1H-isoindol-1-ylidene]amino}phenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

p-aminobenzophenone (99-92-3) + o-phthalic dicarboxaldehyde (643-79-8) → 1-p-acetylphenylimino-2-pacetylphenylisoindoline (60025-39-0)

Guidance literature:

With formic acid; In diethyl ether; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1039/b806544f

Reference yield: 59.0%

p-aminobenzophenone (99-92-3) + 4-nitro-aniline (100-01-6,104810-17-5) + o-phthalic dicarboxaldehyde (643-79-8) → 1-p-acetylphenylimino-2-pacetylphenylisoindoline (60025-39-0) + 1-p-nitrophenylimino-2-p-isopropylphenylisoindoline

Guidance literature:

With formic acid; In methanol; diethyl ether; at 20 ℃; for 12h;

DOI:10.1016/j.ica.2011.09.054

Reference yield:

→ 1-p-acetylphenylimino-2-pacetylphenylisoindoline (60025-39-0)

Guidance literature:

Phthalaldehyd, p-Aminoacetophenon, Me.;

DOI:10.1002/ardp.19763090504

upstream raw materials:

p-aminobenzophenone

o-phthalic dicarboxaldehyde

4-nitro-aniline

Downstream raw materials:

bis(μ-acetato)(1-p-acetophenylimino-2-p-acetophenylisoindoline)dipalladium(II)

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