As(C₆H₅)4⁽¹⁺⁾*OsCl₅C₂H₅OH^(1-)*C₂H₅OH=As(C₆H₅)4OsCl₅C₂H₅OH*C₂H₅OH

Base Information

• Chemical Name: As(C₆H₅)4⁽¹⁺⁾*OsCl₅C₂H₅OH^(1-)*C₂H₅OH=As(C₆H₅)4OsCl₅C₂H₅OH*C₂H₅OH
• CAS No.: 319431-11-3
• Molecular Formula: C₂H₆Cl₅OOs*C₂H₆O*C₂₄H₂₀As
• Molecular Weight: 842.947
• Mol file: 319431-11-3.mol

Synonyms:

Chemical Property of As(C₆H₅)4⁽¹⁺⁾*OsCl₅C₂H₅OH^(1-)*C₂H₅OH=As(C₆H₅)4OsCl₅C₂H₅OH*C₂H₅OH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of As(C₆H₅)4⁽¹⁺⁾*OsCl₅C₂H₅OH^(1-)*C₂H₅OH=As(C₆H₅)4OsCl₅C₂H₅OH*C₂H₅OH

There total 2 articles about As(C₆H₅)4⁽¹⁺⁾*OsCl₅C₂H₅OH^(1-)*C₂H₅OH=As(C₆H₅)4OsCl₅C₂H₅OH*C₂H₅OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

[As(C6H5)4](1+)*[OsCl5(H2O)](1-)*2C2H5OH=[As(C6H5)4][OsCl5(H2O)]*2C2H5OH + ethanol (64-17-5) → As(C6H5)4(1+)*OsCl5C2H5OH(1-)*C2H5OH=As(C6H5)4OsCl5C2H5OH*C2H5OH (319431-11-3)

Guidance literature:

In dichloromethane; Os-complex was dissolved in CH2Cl2, EtOH was added, heated to reflux for 30 min; cooled to 25°C, volatiles were removed; elem. anal.;

DOI:10.1021/ic000084c

Reference yield:

tetraphenylarsonium chloride (507-28-8,14842-08-1) → As(C6H5)4(1+)*OsCl5C2H5OH(1-)*C2H5OH=As(C6H5)4OsCl5C2H5OH*C2H5OH (319431-11-3)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH; H₂SO₄; Na₂SO₃ / water

2: dichloromethane

With KOH; H₂SO₄; Na₂SO₃; In dichloromethane; water;

DOI:10.1021/ic000084c

upstream raw materials:

ethanol

tetraphenylarsonium chloride