2-amino-cyclohex-1-enecarboxylic acid phenethyl-amide

Base Information

Chemical Name:2-amino-cyclohex-1-enecarboxylic acid phenethyl-amide
CAS No.:854133-37-2
Molecular Formula:C₁₅H₂₀N₂O
Molecular Weight:244.337
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-cyclohex-1-enecarboxylic acid phenethyl-amide

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Technology Process of 2-amino-cyclohex-1-enecarboxylic acid phenethyl-amide

There total 6 articles about 2-amino-cyclohex-1-enecarboxylic acid phenethyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 610754-95-5
2-oxo-cyclohexanecarboxylic acid phenethyl-amide

: 854133-37-2
2-amino-cyclohex-1-enecarboxylic acid phenethyl-amide

Guidance literature:: With aluminium trichloride; ammonia; In diethyl ether;
DOI:10.1016/j.bmcl.2005.03.054

Reference yield:

: 854133-16-7
1,4-dioxa-spiro[4.5]decane-6-carboxylic acid phenethyl-amide

: 854133-37-2
2-amino-cyclohex-1-enecarboxylic acid phenethyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. TsOH / acetone / 3 h / 95 °C

2: NH₃; AlCl₃ / diethyl ether

With aluminium trichloride; ammonia; toluene-4-sulfonic acid; In diethyl ether; acetone;
DOI:10.1016/j.bmcl.2005.03.054

Reference yield:

: 4746-93-4
1,4-dioxaspiro[4.5]decane-6-carboxylic acid

: 854133-37-2
2-amino-cyclohex-1-enecarboxylic acid phenethyl-amide

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride / CH₂Cl₂ / 2 h / 20 °C

2: pyridine / 12 h / 20 °C

3: aq. TsOH / acetone / 3 h / 95 °C

4: NH₃; AlCl₃ / diethyl ether

With pyridine; aluminium trichloride; oxalyl dichloride; ammonia; toluene-4-sulfonic acid; In diethyl ether; dichloromethane; acetone;
DOI:10.1016/j.bmcl.2005.03.054