2-benzoyloxy-1-hydroxy-herbertene

Base Information

Chemical Name:2-benzoyloxy-1-hydroxy-herbertene
CAS No.:103412-31-3
Molecular Formula:C₂₂H₂₆O₃
Molecular Weight:338.447
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzoyloxy-1-hydroxy-herbertene

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Technology Process of 2-benzoyloxy-1-hydroxy-herbertene

There total 7 articles about 2-benzoyloxy-1-hydroxy-herbertene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86996-96-5
1,14-dihydroxyherbertene

: 103412-31-3
2-benzoyloxy-1-hydroxy-herbertene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) triphenyl phosphite methiodide, 2.) 5percent aqeous sodium tiosulphate / 1.) HMPA, 3.5 h, room temperature

2: 17 mg / AlCl₃ / 6 h / ice-bath

3: 12 percent / W-4 Raney nickel / ethanol / 1.5 h / Heating

4: 2.) pyridine / 1.) benzene, 90-100 deg C, 1 h, 2.) 4 h, room temperature

With pyridine; aluminium trichloride; triphenyl phosphite methiodide; sodium thiosulfate; W-4 Raney nickel; In ethanol;

Reference yield:

: 86996-94-3
(-)-herbertenolide

: 103412-31-3
2-benzoyloxy-1-hydroxy-herbertene

Guidance literature:: Multi-step reaction with 5 steps

1: 23 mg / LiAlH₄ / diethyl ether / 2 h / ice-bath

2: 1.) triphenyl phosphite methiodide, 2.) 5percent aqeous sodium tiosulphate / 1.) HMPA, 3.5 h, room temperature

3: 17 mg / AlCl₃ / 6 h / ice-bath

4: 12 percent / W-4 Raney nickel / ethanol / 1.5 h / Heating

5: 2.) pyridine / 1.) benzene, 90-100 deg C, 1 h, 2.) 4 h, room temperature

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; triphenyl phosphite methiodide; sodium thiosulfate; W-4 Raney nickel; In diethyl ether; ethanol;

Reference yield:

: 86996-97-6
14-hydroxy-1-methoxyherbertene

: 103412-31-3
2-benzoyloxy-1-hydroxy-herbertene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) triphenyl phosphite methiodide, 2.) sodium cyanoborohydride / 1.) HMPA, 3.5 h, room temperature, 2.) 1.5 h, 70 deg C

2: 17 mg / AlCl₃ / 6 h / ice-bath

3: 12 percent / W-4 Raney nickel / ethanol / 1.5 h / Heating

4: 2.) pyridine / 1.) benzene, 90-100 deg C, 1 h, 2.) 4 h, room temperature

With pyridine; aluminium trichloride; triphenyl phosphite methiodide; sodium cyanoborohydride; W-4 Raney nickel; In ethanol;