4-{(2R,3R,4R,5R)-4-Hydroxy-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester

Base Information

• Chemical Name: 4-{(2R,3R,4R,5R)-4-Hydroxy-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester
• CAS No.: 108802-09-1
• Molecular Formula: C₆₅H₈₆N₂O₁₃
• Molecular Weight: 1103.4

Synonyms:

Chemical Property of 4-{(2R,3R,4R,5R)-4-Hydroxy-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of 4-{(2R,3R,4R,5R)-4-Hydroxy-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester

There total 4 articles about 4-{(2R,3R,4R,5R)-4-Hydroxy-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

9-chloro-9-(4-octadecyloxyphenyl)xanthene (95985-07-2) + 4-{(2R,3R,4R,5R)-4-Hydroxy-5-hydroxymethyl-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester (108782-94-1) → 4-{(2R,3R,4R,5R)-4-Hydroxy-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester (108802-09-1)

Guidance literature:

With pyridine;

DOI:10.1016/S0040-4020(01)88067-4

Reference yield:

Mesitol (527-60-6) → 4-{(2R,3R,4R,5R)-4-Hydroxy-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester (108802-09-1)

Guidance literature:

Multi-step reaction with 2 steps

2: 70 percent / pyridine

With pyridine;

DOI:10.1016/S0040-4020(01)88067-4

Reference yield:

3-methoxy-1,5-dicarbomethoxy-2-pentene (99272-57-8) → 4-{(2R,3R,4R,5R)-4-Hydroxy-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester (108802-09-1)

Guidance literature:

Multi-step reaction with 2 steps

2: 70 percent / pyridine

With pyridine;

DOI:10.1016/S0040-4020(01)88067-4

upstream raw materials:

9-chloro-9-(4-octadecyloxyphenyl)xanthene

4-{(2R,3R,4R,5R)-4-Hydroxy-5-hydroxymethyl-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester

Mesitol

3-methoxy-1,5-dicarbomethoxy-2-pentene

Downstream raw materials:

4-{(2R,3R,4R,5R)-4-[(2-Chloro-phenoxy)-hydroxy-phosphoryloxy]-5-[9-(4-octadecyloxy-phenyl)-9H-xanthen-9-yloxymethyl]-2-[2-oxo-4-(2,4,6-trimethyl-phenoxy)-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yloxy}-4-methoxy-heptanedioic acid dimethyl ester; compound with triethyl-amine

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