N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxamide

Base Information

• Chemical Name: N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxamide
• CAS No.: 936756-53-5
• Molecular Formula: C₂₇H₂₈Cl₃N₃O₃S
• Molecular Weight: 580.963

Synonyms:

Chemical Property of N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxamide

Chemical Property:

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Technology Process of N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxamide

There total 1 articles about N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1λ6-1,2,6-thiadiazine-5-carboxylic acid ethyl ester (936756-39-7) + 1,3,3-trimethylbicyclo[2.2.1]heptan-2-amine (21252-46-0,770696-39-4) → N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1λ6-1,2,6-thiadiazine-5-carboxamide (936756-53-5)

Guidance literature:

With trimethylaluminum; In hexane; dichloromethane; for 24h; Heating;

DOI:10.1016/j.bmc.2007.07.056

upstream raw materials:

2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxylic acid ethyl ester

1,3,3-trimethylbicyclo[2.2.1]heptan-2-amine

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