2-Butenedioic acid, 2-[[3-cyanodihydro-3-[3-methoxy-1-(methoxycarbonyl)-3-oxo-1-propenyl ]-4-phenyl-2(3H)-thienylidene]amino]-, dimethyl ester

Base Information

• Chemical Name: 2-Butenedioic acid, 2-[[3-cyanodihydro-3-[3-methoxy-1-(methoxycarbonyl)-3-oxo-1-propenyl ]-4-phenyl-2(3H)-thienylidene]amino]-, dimethyl ester
• CAS No.: 106118-83-6
• Molecular Formula: C₂₃H₂₂N₂O₈S
• Molecular Weight: 486.502

Synonyms:

Chemical Property of 2-Butenedioic acid, 2-[[3-cyanodihydro-3-[3-methoxy-1-(methoxycarbonyl)-3-oxo-1-propenyl ]-4-phenyl-2(3H)-thienylidene]amino]-, dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Butenedioic acid, 2-[[3-cyanodihydro-3-[3-methoxy-1-(methoxycarbonyl)-3-oxo-1-propenyl ]-4-phenyl-2(3H)-thienylidene]amino]-, dimethyl ester

There total 1 articles about 2-Butenedioic acid, 2-[[3-cyanodihydro-3-[3-methoxy-1-(methoxycarbonyl)-3-oxo-1-propenyl ]-4-phenyl-2(3H)-thienylidene]amino]-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

2-amino-4,5-dihydro-4-phenyl-3-thiophenecarbonitrile (85508-72-1) + dimethyl acetylenedicarboxylate (762-42-5) → 2-Amino-5-cyano-6-phenyl-6,7-dihydro-thiepine-3,4-dicarboxylic acid dimethyl ester (106118-76-7) + (Z)-2-{2-[(Z)-(E)-1,2-Bis-methoxycarbonyl-vinylimino]-3-cyano-4-phenyl-tetrahydro-thiophen-3-yl}-but-2-enedioic acid dimethyl ester (106118-83-6)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; for 24h; Ambient temperature;

DOI:10.1248/cpb.34.396

upstream raw materials:

2-amino-4,5-dihydro-4-phenyl-3-thiophenecarbonitrile

dimethyl acetylenedicarboxylate

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