C₂₇H₅₀N₂O₅Si₂

Base Information

Chemical Name:C₂₇H₅₀N₂O₅Si₂
CAS No.:1567326-66-2
Molecular Formula:C₂₇H₅₀N₂O₅Si₂
Molecular Weight:538.875
Hs Code.:

C<sub>27</sub>H<sub>50</sub>N<sub>2</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₂₇H₅₀N₂O₅Si₂

Chemical Property:

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Technology Process of C₂₇H₅₀N₂O₅Si₂

There total 14 articles about C₂₇H₅₀N₂O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 530-26-7
D-Mannose

: 1567326-66-2
C₂₇H₅₀N₂O₅Si₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: iodine / 16 h / 20 °C

2.1: sodium cyanide / water / 12 h / 50 °C

2.2: 12 h / 20 °C

3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

3.2: 20 h / 20 °C

4.1: acetic acid / water / 3.5 h / 50 °C

5.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

7.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

8.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

9.1: tetrahydrofuran; methanol / 2 h / 20 °C

10.1: potassium carbonate / N,N-dimethyl-formamide

11.1: acetic acid; methanol

12.1: toluene-4-sulfonic acid; trimethyl orthoformate / methanol / 75 °C

13.1: dichloromethane

14.1: toluene-4-sulfonic acid; methanol

With pyridine; methanol; dmap; sodium cyanide; trifluoromethylsulfonic anhydride; iodine; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; triethylamine; triethyl phosphite; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 7757-38-2,14131-84-1,23262-78-4,27108-13-0,33823-04-0,34685-42-2,57819-52-0,78039-08-4,78039-12-0,78964-16-6,94842-76-9,149342-31-4
2,3:5,6-di-O-isopropylidene-D-mannofuranose

: 1567326-66-2
C₂₇H₅₀N₂O₅Si₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium cyanide / water / 12 h / 50 °C

1.2: 12 h / 20 °C

2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

2.2: 20 h / 20 °C

3.1: acetic acid / water / 3.5 h / 50 °C

4.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

6.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

7.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

8.1: tetrahydrofuran; methanol / 2 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide

10.1: acetic acid; methanol

11.1: toluene-4-sulfonic acid; trimethyl orthoformate / methanol / 75 °C

12.1: dichloromethane

13.1: toluene-4-sulfonic acid; methanol

With pyridine; methanol; dmap; sodium cyanide; trifluoromethylsulfonic anhydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; triethylamine; triethyl phosphite; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 137126-24-0
(3aR,4R,7S,7aR)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-7-hydroxy-2,2-dimethyltetrahydro-[1,3]-dioxolo-[4,5-c]-pyran-6-one

: 1567326-66-2
C₂₇H₅₀N₂O₅Si₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

1.2: 20 h / 20 °C

2.1: acetic acid / water / 3.5 h / 50 °C

3.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

5.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

6.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

7.1: tetrahydrofuran; methanol / 2 h / 20 °C

8.1: potassium carbonate / N,N-dimethyl-formamide

9.1: acetic acid; methanol

10.1: toluene-4-sulfonic acid; trimethyl orthoformate / methanol / 75 °C

11.1: dichloromethane

12.1: toluene-4-sulfonic acid; methanol

With pyridine; methanol; dmap; trifluoromethylsulfonic anhydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; triethylamine; triethyl phosphite; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;