{IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}⁽¹⁺⁾*ClO₄^(1-)={IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}ClO₄

Base Information

Chemical Name:{IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}⁽¹⁺⁾*ClO₄^(1-)={IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}ClO₄
CAS No.:148607-57-2
Molecular Formula:C₂₄H₃₆Cl₂IrP₄*ClO₄
Molecular Weight:811.021
Hs Code.:

{IrCl<sub>2</sub>(PH<sub>3</sub>)(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)3}<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>={IrCl<sub>2</sub>(PH<sub>3</sub>)(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)3}ClO<sub>4</sub>

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Chemical Property of {IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}⁽¹⁺⁾*ClO₄^(1-)={IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}ClO₄

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Technology Process of {IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}⁽¹⁺⁾*ClO₄^(1-)={IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}ClO₄

There total 1 articles about {IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}⁽¹⁺⁾*ClO₄^(1-)={IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106587-16-0
{(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄

: 7803-51-2
phosphan

: 148607-57-2
{IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}⁽¹⁺⁾*ClO₄^(1-)={IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}ClO₄

Guidance literature:: In dichloromethane; bubbling PH3 gas through soln. of Ir complex in CH2Cl2; change in color; storage overnight in well ventilated fumehood; addn. of charcoal; stirring suspension under N2 for 60 min;; filtration through Celite; evapn. to dryness under reduced pressure; recrystn. from CH2Cl2/diethyl ether;;
DOI:10.1039/DT9930001093

Reference yield: 71.0%

: 148607-57-2
{IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}⁽¹⁺⁾*ClO₄^(1-)={IrCl₂(PH₃)(P(CH₃)2C₆H₅)3}ClO₄

: 148607-58-3
{IrCl₂(PH₂)(P(CH₃)2C₆H₅)3}

Guidance literature:: With 1,8-diazabicyclo{5.4.0}undec-7-ene; In ethanol; addn. of 1,8-diazabicyclo(5.4.0)undec-7-ene to suspension of Ir complex in ethanol; change in color; stirred vigorously under N2 for 1.5 h;; filtration; washing with ethanol; crystn. from CH2Cl2/ethanol; elem. anal.;;
DOI:10.1039/DT9930001093