1,4-bis(6,6-dicarboxyhexyl)-2,3,5,6-tetramethylbenzene

Base Information

Chemical Name:1,4-bis(6,6-dicarboxyhexyl)-2,3,5,6-tetramethylbenzene
CAS No.:118214-35-0
Molecular Formula:C₂₆H₃₈O₈
Molecular Weight:478.583
Hs Code.:

Synonyms:

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Chemical Property of 1,4-bis(6,6-dicarboxyhexyl)-2,3,5,6-tetramethylbenzene

Chemical Property:

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Technology Process of 1,4-bis(6,6-dicarboxyhexyl)-2,3,5,6-tetramethylbenzene

There total 14 articles about 1,4-bis(6,6-dicarboxyhexyl)-2,3,5,6-tetramethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3022-16-0
1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene

: 118214-35-0
1,4-bis(6,6-dicarboxyhexyl)-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 14 steps

1: 1.) Na / 1.) ethanol; 2.) ethanol, reflux, 0.5 h

2: H₂O, KOH / Heating

3: 94.7 percent / quinoline / 0.33 h / Heating

4: 89.4 percent / cc. H₂SO₄ / toluene

5: 89.6 percent / B₂H₆ / tetrahydrofuran

6: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

7: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

8: H₂O, KOH / Heating

9: 94.6 percent / quinoline / 0.33 h / Heating

10: 95 percent / cc. H₂SO₄ / toluene

11: 99 percent / B₂H₆ / tetrahydrofuran

12: 86 percent / 48 percent HBr / H₂O / 0.5 h / Heating

13: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

14: H₂O, KOH / Heating

With quinoline; potassium hydroxide; sulfuric acid; water; hydrogen bromide; sodium; diborane; In tetrahydrofuran; water; toluene;

Reference yield:

: 3710-01-8
1,4-bis(2-carboxyethyl)-2,3,5,6-tetramethylbenzene

: 118214-35-0
1,4-bis(6,6-dicarboxyhexyl)-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 11 steps

1: 89.4 percent / cc. H₂SO₄ / toluene

2: 89.6 percent / B₂H₆ / tetrahydrofuran

3: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

4: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

5: H₂O, KOH / Heating

6: 94.6 percent / quinoline / 0.33 h / Heating

7: 95 percent / cc. H₂SO₄ / toluene

8: 99 percent / B₂H₆ / tetrahydrofuran

9: 86 percent / 48 percent HBr / H₂O / 0.5 h / Heating

10: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

11: H₂O, KOH / Heating

With quinoline; potassium hydroxide; sulfuric acid; water; hydrogen bromide; sodium; diborane; In tetrahydrofuran; water; toluene;

Reference yield:

: 63134-94-1
1.4-Bis(2.2-bis-aethoxycarbonyl-aethyl)-2.3.5.6-tetramethyl-benzol

: 118214-35-0
1,4-bis(6,6-dicarboxyhexyl)-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 13 steps

1: H₂O, KOH / Heating

2: 94.7 percent / quinoline / 0.33 h / Heating

3: 89.4 percent / cc. H₂SO₄ / toluene

4: 89.6 percent / B₂H₆ / tetrahydrofuran

5: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

6: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

7: H₂O, KOH / Heating

8: 94.6 percent / quinoline / 0.33 h / Heating

9: 95 percent / cc. H₂SO₄ / toluene

10: 99 percent / B₂H₆ / tetrahydrofuran

11: 86 percent / 48 percent HBr / H₂O / 0.5 h / Heating

12: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

13: H₂O, KOH / Heating

With quinoline; potassium hydroxide; sulfuric acid; water; hydrogen bromide; sodium; diborane; In tetrahydrofuran; water; toluene;