{NiI₂py4}

Base Information

• Chemical Name: {NiI₂py4}
• CAS No.: 14077-31-7
• Molecular Formula: C₂₀H₂₀I₂N₄Ni
• Molecular Weight: 628.905
• Mol file: 14077-31-7.mol

Synonyms:

Chemical Property of {NiI₂py4}

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {NiI₂py4}

There total 1 articles about {NiI₂py4} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

nickel(II) iodide (13462-90-3) + bis(pentafluorophenyl)nickel(II) → {NiI2py4} (14077-31-7,14077-10-2) + bis(pentafluorophenyl)bis(pyridine)nickel(II)

Guidance literature:

With pyridine; In not given; pyridine added to a mixture of Ni(C6F5)2 and NiI2; washed with water; recrystd. from CH2Cl2; elem. anal.;

DOI:10.1021/ja00538a058

Reference yield: 73.0%

{NiI2py4} (14077-31-7,14077-10-2) + C51H36F5KN2O2 → C56H41F5IN3NiO2

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 1h; Cooling;

DOI:10.1021/jacs.0c09839

Reference yield: 66.0%

{NiI2py4} (14077-31-7,14077-10-2) + C45H37KN2O2 → C50H42IN3NiO2

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 1h; Cooling;

DOI:10.1021/jacs.0c09839

upstream raw materials:

nickel(II) iodide

Downstream raw materials:

Dibutyl carbonate

di-n-butyl oxalate

tetracarbonyl nickel